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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22895 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-1 Analysis Batch: 720-22967 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22895 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 10 Initial Weight/Volume: 30.02 g <br /> Date Analyzed: 06/21/2007 1938 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/20/2007 1847 Injection Volume: <br /> MSD Lab Sample ID: 720-9514-1 Analysis Batch: 720-22967 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22895 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 10 Initial Weight/Volume: 30.09 g <br /> Date Analyzed: 06/21/2007 2007 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/20/2007 1847 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 67 69 21 - 133 3 35 <br /> Acenaphthene 75 80 40- 145 6 35 <br /> Acenaphthylene 79 76 33- 145 5 35 <br /> Fluorene 71 72 50- 121 0 35 <br /> Phenanthrene 70 76 10- 130 8 35 <br /> Anthracene 77 76 27- 133 2 35 <br /> Benzo[a]anthracene 77 88 33- 143 12 35 <br /> Chrysene 64 79 17- 168 19 35 <br /> Benzo[a]pyrene 55 95 17- 163 42 35 F <br /> Benzo[b]fluoranthene 65 71 24- 159 7 35 <br /> Benzo[k]fluoranthene 55 55 11 - 162 0 35 <br /> Benzo[g,h,i]perylene 83 131 9-219 31 35 <br /> Indeno[1,2,3-cd]pyrene 72 63 9- 171 10 35 <br /> Fluoranthene 68 69 26- 137 2 35 <br /> Pyrene 67 76 52- 115 11 35 <br /> Dibenz(a,h)anthracene 50 101 52- 115 66 35 F F <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 58 71 30- 115 <br /> Terphenyl-d14 82 95 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 188 of 222 06/25/2007 <br />