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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9613-1 <br /> Lab Control Spike/ Method: 8270C <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-22860 Preparation: 3550B <br /> LCS Lab Sample ID:LCS 720-22860/2-A Analysis Batch: 720-22942 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22860 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.17 g <br /> Date Analyzed: 06/20/2007 1607 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1118 Injection Volume: <br /> LCSD Lab Sample ID:LCSD 720-22860/3-A Analysis Batch: 720-22942 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22860 Lab File ID: c:\saturnws\epdata\data\200 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.05 g <br /> Date Analyzed: 06/20/2007 1635 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1118 Injection Volume: <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Naphthalene 59 60 21 - 133 2 35 <br /> Acenaphthene 57 60 40- 145 6 35 <br /> Acenaphthylene 61 62 33- 145 2 35 <br /> Fluorene 63 66 50- 121 5 35 <br /> Phenanthrene 61 59 10- 130 3 35 <br /> Anthracene 63 62 27- 133 1 35 <br /> Benzo[a]anthracene 67 67 33- 143 0 35 <br /> Chrysene 67 66 17- 168 0 35 <br /> Benzo[a]pyrene 65 68 17- 163 6 35 <br /> Benzo[b]fluoranthene 74 77 24- 159 5 35 <br /> Benzo[k]fluoranthene 64 65 11 - 162 2 35 <br /> Benzo[g,h,i]perylene 70 74 9-219 5 35 <br /> Indeno[1,2,3-cd]pyrene 78 80 9- 171 3 35 <br /> Fluoranthene 61 63 26- 137 3 35 <br /> Pyrene 64 65 52- 115 2 35 <br /> Dibenz(a,h)anthracene 78 78 9- 171 0 35 <br /> Surrogate LCS% Rec LCSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 63 66 30- 115 <br /> Terphenyl-d14 69 69 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 19 of 25 06/28/2007 <br />