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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9613-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22860 Preparation: 3550B <br /> MS Lab Sample ID: 720-9613-1 Analysis Batch: 720-22942 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22860 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 1.0 Initial Weight/Volume: 30.30 g <br /> Date Analyzed: 06/20/2007 1900 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1118 Injection Volume: <br /> MSD Lab Sample ID: 720-9613-1 Analysis Batch: 720-22942 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22860 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Initial Weight/Volume: 30.40 g <br /> Date Analyzed: 06/20/2007 1928 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/20/2007 1118 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 57 57 21 - 133 0 35 <br /> Acenaphthene 57 55 40- 145 3 35 <br /> Acenaphthylene 56 57 33- 145 2 35 <br /> Fluorene 62 60 50- 121 4 35 <br /> Phenanthrene 56 57 10- 130 1 35 <br /> Anthracene 59 60 27- 133 1 35 <br /> Benzo[a]anthracene 66 63 33- 143 5 35 <br /> Chrysene 64 63 17- 168 2 35 <br /> Benzo[a]pyrene 61 62 17- 163 0 35 <br /> Benzo[b]fluoranthene 69 68 24- 159 1 35 <br /> Benzo[k]fluoranthene 57 60 11 - 162 4 35 <br /> Benzo[g,h,i]perylene 63 65 9-219 3 35 <br /> Indeno[1,2,3-cd]pyrene 72 72 9- 171 1 35 <br /> Fluoranthene 59 59 26- 137 0 35 <br /> Pyrene 62 62 52- 115 1 35 <br /> Dibenz(a,h)anthracene 71 73 52- 115 2 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 61 60 30- 115 <br /> Terphenyl-d14 66 65 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 20 of 25 06/28/2007 <br />