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CURTIS & TOMPKINS INITIAL CALIBRATION FOR 218019 PEST Soil : EPA 8081A Inst : GC23 Name : gc23 PEST 031 Calnum : 800046786001 Date : 01-FEB-2010 15 : 05 Units : pg/uL Level File Seqnum Sample TD Analyzed Stds L1 031_010 800046786010 PEST 1 01-FEB-2010 15:05 513884 L2 031_011 800046786011 PEST_2 01-FEB-2010 15:28 513885 L3 031_012 800046786012 PEST_3 01-FEB-2010 15:50 513886 L4 031_013 800046786013 PEST_4 01-FEB-2010 16:12 513887 L5 031_014 800046786014 PESTS 01-FEB-2010 16:34 513888 L6 031_013 800046786015 PEST_6 01-FEB-2010 16:57 513889 L7 031_016 800046786016 PEST_7 01-FEB-2010 17:19 513890 r^2 Analyte h Ll L2 L3 L4 L5 L6 L7 Type X a0 al a2 Avg %RSD MnR^2 MxRSD Flg alpha-BHC A 10177 9482.0 9546.2 9683.4 10062 10994 AVRG R 1.00E-4 9990.8 6 0.990 20 gamma-BHC A 9881.0 8971.2 8932.9 8835.1 9103.8 9914.2 AVRG R 1.08E-4 9273.0 5 0.990 20 beta-BHC A 4350.0 3806.8 3789.6 3470.2 3617.4 3358.7 3678.2 AVRG R 2.68E-4 3724.4 9 0.990 20 delta-BHC A 8959.5 7894.4 7938.1 7776.9 8119.6 9031.4 AVRG R 1.21E-4 8286.7 7 0.990 20 Heptachlor A 8375.5 7788.0 8035.9 7812.7 8201.6 8846.6 AVRG R 1.22E-4 8176.7 5 0.990 20 Aldrin A 9424.5 8684.0 8602.4 8417.1 8755.8 9338.4 AVRG R 1.13E-4 8870.4 5 0.990 20 Heptachlor epoxide A 8430.5 7917.4 7700.6 7423.4 7637.0 8043.5 AVRG R 1.27E-4 7858.7 5 0.990 20 gamma-Chlordane A 8090.0 7308.6 7302.6 7176.5 7369.1 7699.8 AVRG R 1.33E-4 7491.1 5 0.990 20 alpha-Chlordane A 7895.5 7169.0 7111.7 6908.9 7140.5 7419.2 AVRG R 1.37E-4 7274.1 5 0.990 20 4,4'-DDE A 6246.8 5934.7 5999.3 6025.9 6346.2 7639.0 8803.5 QUAD A -9579.7 6177.03 13.46238 6713.6 1.000 0.990 20 Endosulfan T A 7589.5 6969.2 6963.4 6856.9 7035.5 7281.7 AVRG R 1.41E-4 7116.0 4 0.990 20 Dieldrin A 8553.0 7356.1 7450.5 7733.9 8152.5 10251 9011.7 QUAD A -51090 10669.5 -6.68396 8358.4 0.994 0.990 20 Endrin A 6322.3 5680.7 5687.3 5796.4 6267.5 7966.8 8019.9 LTNR R 6.02026 1.22E-4 6534.4 0.996 0.990 20 4,4'-DDD A 4348.5 4071.0 4070.6 4254.1 4403.7 5539.0 7180.9 QUAD A -942.94 3725.58 17.33755 4838.3 1.000 0.990 20 Endosulfan TT A 7302.8 6353.6 6694.5 6708.0 7036.2 8258.6 AVRG R 1.42E-4 7058.9 10 0.990 20 4,4'-DDT A 3994.3 3949.0 4248.3 4388.7 4660.1 6009.0 7525.5 QUAD A -8780.7 4277.41 16.53031 4967.8 1.000 0.990 20 Endrin aldehyde A 5356.0 4521.0 4731.5 4652.9 4759.3 5343.7 AVRG R 2.04E-4 4894.1 7 0.990 20 Methoxychlor A 1959.7 1846.8 1800.4 1931.9 2150.8 3139.9 QUAD A 26618.6 1005.51 4.159063 2138.2 1.000 0.990 20 Endosulfan sulfate A 5348.3 5002.4 5068.8 5078.2 5252.7 6153.5 AVRG R 1.88E-4 5317.3 8 0.990 20 TCMX A 6165.8 5822.6 5852.9 5816.1 5851.4 6025.9 AVRG R 1.69E-4 5922.4 2 0.990 20 Decachlorobiphenyl A 6026.8 5968.1 5673.2 5527.1 6608.4 5948.5 7240.6 AVRG R 1.63E-4 6141.8 10 0.990 20 alpha-BHC B 30680 27181 26570 26009 23991 22299 LTNR R -1.8608 4.57E-5 26122 0.996 0.990 20 gamma-BHC B 25398 23464 22853 22170 20480 19179 AVRG R 4.49E-5 22257 10 0.990 20 beta-BHC B 11600 10485 9820.9 9553.8 8793.3 9291.4 8231.2 LTNR R -2.2658 1.22E-4 9682.2 0.996 0.990 20 delta-BHC B 25128 22563 21647 20744 19063 18391 LTNR R -1.6245 5.56E-5 21256 0.998 0.990 20 Heptachlor B 24944 23539 22923 22105 20108 18622 13552 QUAD A 3524.60 23273.6 -97.4657 20827 0.999 0.990 20 Page 1 of 4 800046786001 81 of 295