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r^2 Analyte mi Ch T L3 L4 L6 L7 Type X a0 al a2 Avg %RSD MnR^2 MxRSD Elg Aldrin B 24479 22780 21961 20847 19128 17311 12565 QUAD A 8217.32 21698.4 -92.1266 19867 1.000 0.990 20 Heptachlor epoxide B 20853 21497 19381 18101 16273 15083 10731 QUAD A 9319.35 18816.0 -81.6704 17417 0.999 0.990 20 gamma-Chlordane B 22804 21598 19240 17787 15885 15127 LINR R -2.5480 6.86E-5 18740 0.996 0.990 20 alpha-Chlordane B 19140 18966 17613 16559 14921 14218 LINR R -2.1155 7.23E-5 16903 0.996 0.990 20 4,4'-DDE B 16738 17794 16377 15003 13150 11924 7572.8 QUAD A 15792.4 15754.8 -41.2619 14080 0.998 0.990 20 Endosulfan I B 18647 18418 17122 16091 14383 13796 LINR R -2.1198 7.46E-5 16409 0.996 0.990 20 Dieldrin B 19619 19314 17727 15257 13303 10601 6685.1 QUAD A 58701.2 14247.4 -39.4218 14644 0.996 0.990 20 Endrin B 15191 14955 13964 12407 10987 9204.5 5948.9 QUAD A 31883.6 12222.5 -32.2265 11808 0.998 0.990 20 4,4'-DDD B 12709 14047 12985 11883 10464 10127 6767.7 QUAD A 2783.43 12897.9 -30.6216 11283 0.998 0.990 20 Endosulfan II B 16729 15974 14807 13073 11436 9765.4 6330.4 QUAD A 35329.1 12820.1 -33.3761 12588 0.998 0.990 20 4,4'-DDT B 13929 14056 13125 11978 10606 9744.5 6282.6 QUAD A 10294.5 12739.4 -32.4891 11389 0.998 0.990 20 Endrin aldehyde B 12878 11605 11096 9949.9 8716.1 8168.2 5338.0 QUAD A 11263.3 10491.2 -25.9885 9678.8 0.998 0.990 20 Methoxychlor B 5440.3 5314.6 4748.2 3718.0 3156.9 2416.3 1453.6 QUAD A 112560 3229.77 -1.89769 3749.7 0.990 0.990 20 Endosulfan sulfate B 12739 12178 11433 10265 8949.9 8141.2 5340.6 QUAD A 16711.6 10521.2 -26.2972 9863.9 0.998 0.990 20 TCMX B 15167 14394 13978 13702 13155 12523 AVRG R 7.24E-5 13820 7 0.990 20 Decachlorobiphenyl j B 9488.5 9245.3 8925.0 7817.1 6609.8 6786.0 4552.1 QUAD A 4079.05 8412.35 -19.3034 7632.0 0.995 0.990 j 20 Average EPA 8081A A (n=23) 1 10 1 1 20 Average EPA 8081A B (n=23) 1 21 1 20 arsd *** Page 2 of 4 800046786001 82 of 295