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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 a Sparks, Nevada 89431 -5778 <br /> (775) 355-1044 a (775) 355-0406 FAX • 1-800-283- 1183 <br /> Date: QC Summary Report W14 30442 <br /> 13-Mar-14 <br /> Method Blank Type MBLK Test Code: EPA Method SW60201 SW6020A <br /> File ID: 030_ - Batch IDi 32532 Analysis Date: 031051201411 :42 <br /> Sample ID: MB-32532 Units : mg/Kg Run ID: ICPIMS_1403058 Prep Date: 031041201414:49 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVaI %RPD(Limit) Qual <br /> Lead (Pb) - ND 1 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW6020I SW6020A <br /> File ID: 032_ Batch ID: 32532 Analysis Date: 031051201411 :48 <br /> Sample ID: LCS42532 Units ; mglKg Run ID: ICPIMS_140306B Prep Date: 031041201414:49 <br /> AnaVe - Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Llmit) - Qual <br /> Lead (Ph) 25.6 1 25 102 80 120 - <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW6020I SW6020A <br /> File ID: 034_ Batch ID: 32532 - Analysis Date: 031051201411 :54 <br /> Sample ID: 1402272241AMS Units : mglKg Run ID: ICPIMS 1403058 Prep Date: . 031041201414:49 <br /> Analyte - Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Lead (Pb) 33.1 1 25 9.715 94 . 75 125 <br /> Sample Matrix Spike Duplieate Type MSD Test Code: EPA Method SW60201 SW6020A <br /> File ID: 035_ Batch ID: 32532 Analysis Date: 03105/2014 11 :57 <br /> Sample ID: 14022722-01AMSD Units : mglKg Run ID: ICPIMS_140305B Prep Date: 031041201414:49 <br /> Analyte, Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Llmit) Qual <br /> Lead (Pb) 34.5 1 25 9.715 99 / 75 125 33.15 - 4.1(20)- <br /> Comments: <br /> Calculations are based off of raw (non-rounded) data However, for reporting purposes, all QC data is rounded to three significant figures. Therefore, hand calculated <br /> values may differ slightly. - - <br />