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II <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 3554044 9 (775) 355-0406 FAX • 1-800-283-1183 <br /> Da"' QC Summary Report w1aiaaz" <br /> 16-MM44 <br /> Method Blank Type MBLK Test Code: EPA Method SWB016WC ISWO260B <br /> File 10: 14030808,0 Batch ID: msoBS2640B Analysis Date: 03MW201413:07 <br /> Sample ID: MBLK MS0BS25400 Units : mglKg Run ID: MSD 08_140306A Prep Data: 0IMW201413:07 <br /> Analyte - Result PQL SpkVal Spk sl %REC LCL(ME) UCL(ME) RPDReNaI %RPD(Umft) Quel <br /> TPH-P (GRO) NO 1 <br /> Bun: 1 ,2-Dichlorosthane-d4 0.22 0.2 110 70 130 <br /> Sum Toluene-dB 0.209 0.2 104 70 130 <br /> Sum 4-BromoBuorobenzene 0.199 0.2 99 70 130 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method 311111801661C ISW82803 - - <br /> File ID: 14030625.D Batch ID: M30852540B Analysis Date: 031081201421 :01 <br /> Sample ID: GLCS MS08826408 Units : mg1Kg Run ID: MSD_08_140306A Prep Date: 031061201421 :01 <br /> Analyte Result POL SpkVal SpkReMal %REC LCL(ME) UCL(ME) RPDReNaI %RPD(Limlt) Qual <br /> TPH-P (GRO) 15.2 - 2 16 - 95 63 149 <br /> Surf: 1 ,2-Dichlomelhaned4 0.4 0.4 99.9 70 130 <br /> Bum Toluene-d8 0.351 0.4 88 70 130 <br /> Sun: 443romo0uorobenzene 0.512 0.4 128 70 130 <br /> Sample Matrix Spike - Type MS Test Cade: EPA Method SW11016B1C / SW62608 <br /> File ID: 14030628.D Batch ID: MSOBS2640B Analysis Date: 031061201421 :26 <br /> Sample 10: 14030442-01AGS Units : mil Run ID: MSD08140306A . Prep Date: 031081201421 :26 - <br /> Analyte Result PQL SpkVal SpkRelVal %REC LCL(ME) UCL(ME) RPDReNaI %RPD(Umlt) Qual - <br /> TPH-P (GRO) 15.5 2 1s 0 97 36 - 164 <br /> Sun: 1 ,2-Olchloroethaned4 0.379 0.4 95 70 130 <br /> Sum Toluenad8 - 0.355 0.4 69 70 130 S55 <br /> Sum 4-Bromoftuorobenzens 0.529 0.4 132 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SWeolinuCISW62606 <br /> File 10: 14030627.0 Batch ID: 1111508325400 Analysis Dale: 03IM201421 :51 <br /> Sample ID: 140304112.OtAG30 Units : mglKg Run ID: 41180j8140306A Prep Oslo: - 031061201421 :51 <br /> Analyte Result PCIL SpkVal SpkReP/el %REC LCL(ME) UCL(ME) RPORe1Val %RPD(UnrlQ Qual <br /> VH-P (GRO) 14.5 2 16 0 90 36 164 - 15.45 _ 6.8(40) <br /> Sum 1 ,2-Dichioroethened4 0.366 0.4 92 70 130 <br /> Sum Toluene-d8 0.356 0.4 89 70 130 S55 <br /> Surr: 4-BromcBuoroberwene 0.528 0.4 132 70 130 <br /> Comments: - <br /> Calculations are based off of raw (non-rounded) data. However, for reporting purposes, no QC data is rounded to am significant figures. Therefore, hand calculated <br /> values may differ slightly, _ <br /> S55 a Surrogate recovery was above laboratory acceptance limits. <br /> I <br />