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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 • Sparks,Nevada 89431-5778 <br /> I� (775)355-1044 • (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: <br /> 14-May-02 QC Summary Report work Order: <br /> 02050321 <br /> Method$lank Type MBLK Test Code:SW8015 Batch ID:MS4W0506B <br /> File ID:C:IHPCHEM1MS041DATA1020506102050607.D Analysis Date: 05/06/2002 11:29 <br /> Sample ID: MBLK MS4W0506AlB Units:mg/L Run ID:GCIMSD_4 020506A Prep Date: 05/06/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND 0.05 <br /> Surr: 1,2-Dichloroethane-d4 0.00942 0.01 94 71 130 <br /> Surr:Toluene-d8 0.0104 0.01 104 69 127 <br /> Surr:4-Bromofluorobenzene 0.0115 0.01 115 80 123 <br /> Laboratory Control Spike Type LCS Test Code:SW8015 Batch ID:MS4W0506B <br /> File ID:C:kHPCHEM1MS041DATA1020506102050606.D Analysis Date: 05/06/2002 11:06 <br /> Sample ID: CVIGLCS MS4W0506B Units:mg/L Run ID:GCIMSD_4_020506A Prep Date: 05/06/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 0.402 0.05 0.4 101 58 136 <br /> Surr: 1,2-Dichloroethane-d4 0.00938 0.01 94 71 130 <br /> Surr:Toluene-d8 0.0103 0.01 102 69 127 <br /> Surr;4-Bromofluorobenzene 0.0112 0.01 112 80 123 <br /> Sample Matrix Spike Type MS Test Code:SW8015 Batch ID:MS4W0506B <br /> File ID:C:IHPCHEM1MS04kDATA1020506102050610.D Analysis Date: 05/06/2002 12:45 <br /> Sample ID: 02050321-OIAGS Units: mg/L Run ID:GC/MSD_4 020506A Prep Date: 05/0612002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 2.09 0.25 2 0 100 58 136 <br /> Surr, 1,2-Dichloroethane-d4 0.0469 0.05 94 71 130 <br /> Surr:Toluene-d8 0.0533 0.05 107 69 127 <br /> Adlfiurr-4-Bromofluorobenzene 0.0557 0.05 111 80 123 <br /> ample Matrix Spike Duplicate Type MSD Test Code:SW8015 Batch ID:MS4W0506B <br /> File ID:C:IHPCHEMkMS04kDATA1020506102050611.D Analysis Date: 05/06/2002 13:08 <br /> Sample ID: 02050321-01AGSD Units: mg/L Run ID:GCIMSD_4 020506A Prep Date: 05/0612002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-im€t HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 2.1 0.25 2 0 105 58 136 2.01 4.6 <br /> Surr:1,2-Dichloroethane-d4 0.0464 0.05 93 71 130 <br /> Surr:Toluene-d8 0.0518 0.05 104 69 127 <br /> Surr:4-Bromofluorobenzene 0.0563 0.05 113 80 123 <br /> Comments: ND-Not Detected at the Reporting Limit. D-If the spiked value is X25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br /> i <br />