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Alpha Analytical, Inc. <br /> { 255 Glendale Ave. •Suite 21 • Sparks, Nevada 89431-5778 <br /> I�. (775)355-1044 • (775)355-0406 FAX• 1-800-283-1183 <br /> Date: <br /> 14-Mrsy-02 QC Summary Report 'Fork Order: <br /> 02054321 <br /> Method ]Blank Type MBLK Test Code:5W$260B <br /> File ID:C:IHPCHEMIMSO4IDATA1O2O506102050607.D Batch ID:MS4WO506A <br /> Sample ID: MBLK MS4WO506AIBAnalysis Date: 05/06/2002 11:29 <br /> Analyte <br /> Units:Ng1L Run lb:GCINISD 4 020506A Prep Date: 0510612002 <br /> Result PQL SpkVal SpkRefVal /oREC LowLhLimit RPD Ref Val <br /> 9 °tmit Hi /oRPD <br /> Tertiary Butyl Alcohol(TBA) ND ° Qual <br /> 5 <br /> Methyl tert-butyl ether(MTBE) ND <br /> Di-isopropyl Ether(DIPE) 0.5 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1 <br /> Benzene <br /> Tertiary Amyl Methyl Ether AME ND 0.5 <br /> Toluene y ) ND 1 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> ND 0.5 <br /> 9 <br /> Surr: 1,2-Dichloroethane-d4 .42 14 94 71 130 <br /> Surr:Toluene-d8 10.4 1D 104 fig 127 <br /> Surr:4-Bromofluorobenzene 11.5 10 115 80 123 <br /> Laboratory Control Spike Type LCS Test Code:SW8260B <br /> File ID:C:IHPCHEM1MSO41DATA10205061420506O5.D Batch 1D: ate: 0506A <br /> Sample ID: CVILCS MS4WO506A Units : Analysis Date: 05/06/2002 10:43 <br /> NgIL Run ID:GCIMSD_4_02D506A Prep Date: 05/06/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLhl-imit RPD Ref Val /oRPD <br /> g °tmit Hi <br /> Benzene ° Qual <br /> Toluene 10.4 0.5 10 104 80 120 <br /> 10.6 0.5 10 106 80 120 <br /> Ethylbenzene <br /> m 10.5 0.5 10 105 80 120 <br /> X Xylene 21.6 0.5 20 108 73 129 <br /> WXylene 10.8 0.5 10 108 73 127 <br /> rr: 1,2-Dichloroethane-d4 9.47 10 95 71 ,. <br /> rr:Toluene-d8 10.2 130 <br /> 10 102 69 127 <br /> Surr:4-Bromofluorobenzene <br /> 10.3 10 103 80 123 <br /> Sample Matrix Spike Type MS Test Code:SW82606 <br /> File ID: C:IHPCHEM1MSO41DATA1020506102050608.D Batch ID:MS4W0506A <br /> Sample ID: 02050321-OIAMSAnalysis Date: 05/06/2002 11:58 <br /> Units: NgIL Run !D:GCIMSD 4 020506A Prep Date: 05/06/2002 <br /> Analyte <br /> Toluene Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Quai Toluene 51.2 1.3 50 0 102 80 120 Ethylbenzene 51.7 1.3 50 0 103 80 120 <br /> m,p-Xylene 52.6 1.3 50 0 105 80 120 <br /> o-Xylene <br /> 106 1.3 100 0 106 73 129 Sur52.4 1.3 50 0 105 73 127 <br /> Surr 1,2-Dichloroethane-d4 47 50 <br /> Surr:Toluene-d8 94 71 130 <br /> 50.1 50 100 69 127 <br /> Surr:4-Bromofluorobenzene 50.8 50 <br /> 102 80 123 <br /> Sample Matrix Spike DupIicate Type MSD Test Code:SW82608 <br /> File 1D: C:IHPCHEMIMSO4IDATA1020506102050609.D Batch ID:MS4WO506A <br /> Sample 1D: 02050321-01AMSDAnalysis Date: 05/06/2002 12:22 <br /> Units:pglL Run ID:GCIMSD_4_020506A Prep Date: 05/06/2002 <br /> Analyte <br /> Benzene Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> 50.8 1.3 50 <br /> Toluene 50.1 1.3 50 0 102 80 120 51.18 0.804 <br /> 0 100 80 120 <br /> Ethylbenzene 51.2 1.3 50 0 102 80 120 51.67 3.43 <br /> m,p-Xylene _ 102 1.3 100 52.55 2.7 <br /> o-Xylene 0 102 73 129 105.8 394 <br /> Surr: 1,2-Dichloroethane-d4 51.4 1.3 50 0 103 73 127 52.42 1,89 <br /> 48.8 50 98 71 130 <br /> Surr:Toluene-d8 50.1 50 <br /> Surr:4-Bromofluorobenzene 100 69 127 <br /> 50.9 50 <br /> 102 80 123 <br /> �mments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br />