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110 2nd Avenue South,0137,Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, 1'elephone:925-798-1620 Fax:925-798-1622 <br /> 14, Website:www.mccanipbcIl com E-mail miun`cSmccarripbellconr <br /> Advanced GeoEnvironmental, Inc. Client Project ID: National Freight Date Sampled: 12/I7/03 <br /> 837 Shaw Road Date Received: 12/18/03 <br /> Client Contact: Paul Dotson Date Extracted: 12/20/03 <br /> Stockton, CA 95215 <br /> Client P.O.: Date Analyzed: 12/20/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method: SW5030B Analytical Method:SW8260B Work Order.0312365 <br /> Lab ID 0312365-001B 0312365-002B 0312365-003B 0312365-004B <br /> Client ID MWI/121703 MW2/121703 MW3/121703 MW4/121703 <br /> Reporting Limit for <br /> Matrix W- -W W W DF=I <br /> 71 10 - 1 - 1 I S W <br /> Compound Concentration ug/kg pg/L <br /> ten-Amyl methyl ether(TAME) ND<5.0 ND ND ND NA { 0.5 <br /> t-Butyl alcohol(TBA) ND<50 ND ND ND NA 5.0 <br /> 1,2-Dibromocthane(EDB) ND<5.0 ND ND i ND NA 0.5 <br /> 1,2-DLchloroc1hane(1,2-DCA) ND<5.0 -- ND ND - ND - - NA 0.5 <br /> Diisopropyl ether(DIPS) ND<5.0 ND ND NO NA 0.5 <br /> Ethanol ND<500 ND ND — ND NA 10 <br /> Gtl,vl tcri-butyl cther(ETBF) ND<5.0 ND ND ND NA }.5 <br /> Methano; ND<5000— ND ND ND NA 500 <br /> Methyl-t-butyl ether(IMTB>) ND<5.0 ND ND - --ND -- NA 0.5 <br /> Surrogate Recoveries <br /> 96.7 103 104 l 04 <br /> Comments -_ j,h,i i i <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludgelsolid samples in pg/kg, wipe samples in uylwipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> 9 surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheenlproduct is present;i)liquid sample that contains greater than--2 vol.%sediment;j)sample diluted due to high <br /> or anic content. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />