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r Inc. 10 2nd Avenue Sauth,ttD7,Pacheco,CA 945 53-5 560 <br /> McCampbell Analytical, nc. Telephone:925-798-1620 fax:925-798-1622 <br /> -4 Website:www.mccamphdl,com E-mail:mam',alniccampbell.coni <br /> Advanced GeoEnvironmental, Inc. Client Project ID: National Freight Date Sampled: 12/17/03 <br /> 837 Shaw Road Date Received: 12/18/03 <br /> Client Contact: Paul Dotson Date Extracted: 12/20/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 12/20/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GCIMS* <br /> Fxtraction Method: SW5030B Analyiicai Method:SW8260B Work Order:0312365 <br /> Lab ID 0312365-0058 <br /> Client ID MW5/121703 <br /> Reporting Limit for <br /> Matrix .— W �— ---- --- DF-1 <br /> F- 1 g W <br /> Compound Concentration inks 4g/L <br /> tert-Amyl methyl ether(TAME) ND NA 0.5 <br /> t-Butyl alcohol(TBA) ND —NA 5.0 <br /> 1,2-Dibromoethane(EDB) ND NA 0.5 <br /> 1,2-Dichlorocthanc(I.2-DCA) ND NA 0.5 <br /> Diisopropyl ether(DIPL) ND NA 0.5 <br /> Ethanol ND VA 50 <br /> Ethyl Cert-butyl ether ND j `,A o.5 <br /> i <br /> Methanol ND NA 100 <br /> Methyl-t-butyl ether(MTBE) ND NA 0.5 <br /> Surrogate Recoveries <br /> %S5: 104 - <br /> I <br /> Comments i <br /> *water and vapor samples and all-I CLP&SPLP extracts are reported in gg/L,soii'sludge'solid samples inµglkg, wipe samples inµglwipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted nut of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than -2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />