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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> bttpi//www.mccampbell.com E-mail: main@mccampbell.com <br /> Advanced Geo Environmental Client Project ID:National Freight Date Sampled: 08114-08/15100 <br /> 4005 North.Wilson Way Date Received: 08/18/00 <br /> Stockton, CA 95205 Client Contact:Tim Cuellar Date Extracted: 08/18/00 <br /> Client P.O: Date Analyzed: 08/21-08/22/00 <br /> i <br /> 7 Oxygenated Volatile Organics By GUMS <br /> FPA method 8260 modified <br /> Lab ID 45266 45267 45268 45269 <br /> Reporting Limit <br /> Client ID P3-75 P3-80 P3-90 P3-100 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg uglL <br /> Di-isopropyl Ether(DIPS) ND ND ND ND 5.0 1.0 <br /> ----------------- <br /> Ethyl ter -Butyl Ether(ETBE) ND ND ND ND 5.0 lA <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromolluoromethane 101 99 97 97 <br /> Comments: <br /> — *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscibie sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />