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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL .A.NALYTICAL INC. Telephone:925-798-1620 Fax : 925-798-1622 <br /> http://www,mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:National Freight Date Sampled: 08/14-08115/00 <br /> 4005 North Wilson Way Date Received: 08/18/00 <br /> Stockton, CA 95205 Client Contact: Tim Cuellar Date Extracted: 08/18/00 <br /> Client P.O: Date Analyzed: 08/21-08/22/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 45274 45275 45276 45277 <br /> Reporting Limit <br /> Client ID MW1-60 MW1-75 MW2-10 MW2-20 <br /> Matrix S S IL 11 5 S S w <br /> Compound Concentration* ug/kg ug/L <br /> Di isopropyl Ether(DIFF) ND ND ND ND 5.0 1.0 <br /> Ethyl tett-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND �NDND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries{%) <br /> Dibromolluoromethane 97 96 92 93 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samp€es in ug/kg,wipes in ug/wipe and all TCLP 1 STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No, 1644 Edward Hamilton, Lab Director <br /> 5 <br />