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ODENWHRO-TEICH CERTIFICATE OFANA LYSIS <br /> Analytical Laboratory <br /> Friday,July 02, 1999 <br /> Advanced Geo Environmental <br /> 4005 N. Wilson Way <br /> Stockton, CA. 95205 <br /> Sample Information <br /> Sample]D: PE5380-03 SampleTjpe: Grab <br /> Sample Description: B2 @ 15' Project Name. ACME SAW&INDUSTRIAL <br /> Date/Time Sampled: 6/15/99 9:48:00 AM Sample MatrLr: Soil <br /> ANALYTICAL RESULT QAIQC <br /> REPORT h <br /> 4 <br /> .........:::::::..:;::::•:•+:•:......::::::::»::::+.:-::.::.:-r:C.......:::;»::.::.::::::::::......::::::::::::nw::::::::::x:n..........n-:::::n:•.r.:..v:n,w::::::::::x:::::xnvnvw::::::::::nw.::::::n�::::::::::::::::::..C,••>;oy.,,w.�.,w::::::.x:•iY:•.:.;.:.:rn:.y::.l-.Y-:rx:nEn;:::::::•y::p:.::np�.,;.::.•.::>Y•:::.•yn-:::n,-.Y::.x-:.�:n:•nn„••r?�:.;.:•;.�:•:�•..:xyxti <br /> Date LCS Spike MS Spike <br /> - Test Parameter Method DLR Unit Result Dilution :Analyzed S% S% <br /> Blank' M MSD RSD <br /> Conc. LC Conc. <br /> #i TPH-Gasoilne EPA 8015M/DHS 1 mg/Kg ND 1 17-Jun-99 ND 2 97.5° 2 90.0°%o 87.5% 0.7% <br /> TPH Diesel EPA 8015M/DHS 1 mg/Kg ND 1 <br /> 17-Jun-99 ND 50 94.0% 50 86.0% 84.0% 0.6% a <br /> ` EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 84.0 5 80.0% 82.0° 0.6� <br /> Benzene ° ° <br /> �'�, ;...... ............ . .... ............ ...... .. <br /> ;Toluene EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND ........,•5.•... 98.00/0 5.,•. 98.00/6 1.0%: <br /> Ethylbenzene EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 102.0°/6 5 80.00/0 92.0% 3.5% <br /> ” Xylenes Total EPA 8020 5 ug/Kg ND 1 17 Jun 99 ND 10 92.0% 10 91.0% 90.00/0 <br /> ` ;Methyl-t-Butyl Ether(MtBE) EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 92.0°k 5 84.0% . 86.0% 0.6°/0 <br /> =milligrams per Liter=ppm DLR-Detection Limit for the Purpose of RSD-represent relative percent different(RPD)between duplicates spike ofsanlples <br /> ag11-=micrograms peri iter=ppb Reporting. F,xceptional sample matrices or or Duplicate of Sample <br /> interferenece:s may result in higher detection MSAILM-measure of 1 the percent recovery efficiencies within the matrix <br /> " C=Composite G=Grab limits <br /> LCS-measure ofthe percent recovery ofthe Laboratory Control Spike(LCS) <br /> .1 . <br /> RESPEC FULL B ITTED, <br /> Jonathan Hao V. Le, Laboratory Director <br /> .......... „:::......,....................................,,,,......:,:,,...:::,:,,:.......................... <br /> ..............,...:..,...............,.:............,,....,.....:............................:..:...............:..:..:....:.. . <br /> EPA-13nvirortntental ProtectiotiAgeneydlethod. Page I of 1 <br /> SM-ElandardrDfethodfot•Exar»inaliondSW8eElriC4&VellfOdc6t. Suite A Stockton, CA 95204 Tel.: (209) 462-0892 Fax: (209) 462-7935 <br />