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(C 0.5 00 H <br /> CERTIFICATE OFANALYSIS <br /> Ana/ytica/ Laboratory <br /> friday, July 02, 1999 <br /> Advanced Geo Environmental <br /> 4005 N. Wilson Way <br /> Stockton, CA. 95205 <br /> k <br /> Sample Information <br /> Sample ID: PE5380-04 Sample Type: Grab <br /> Sample Description: B2 @ 30' Project Name: ACME SAW.&INDUSTRIAL <br /> Date/Time Sample& 6/15/99 10:15:00 AM Sample Matrix: Soil <br /> Ac <br /> ti ANALYTICAL RESULT :: ,..............,,......:,...;,...,....,. <br /> r <br /> QA/QC REPORT <br /> 4 <br /> � ::::nw::.:::.:::::::::::::::.::::::::::.v.v::.w;..:....::::::::::..::..::::::..... ...::::......:::nn.. ...w:;;.• '.:,,..... ............. v....v:v;::n:+::.v::n•:.tt••ivn»;:.+:{G..Ui,•.ttv:n•:m:n;.::,;.ttttt::::.v.:t\}\bY'.,,\., is\. <br /> Date LCS Spike MS Spike s <br /> Test Parameter Met/cod DLR Unit Result Dilution Analyzed on <br /> Blank C c. LCS% Cotte MS% MSD RSD <br /> TPH Gasoline EPA 8015M/DHS 1 mg/Kg ND 1 17-Jun-99 ND 2 97.5°t6 2 90.0°� 87.5% 0.7% <br /> ' ...:.v::•?w..:::::::::::.:::::::::::::::.::::::::::: :.: :..:::..:.:.v::::::::::.;+,:.n.::::;;, ... .:.:::::::::.:.......:. ..:.: ..::;:::::::::..:.v:nttw::,y.v.:::::.v:..w::::::..::::::::n,w:::w:.w.::.:.v.»,v:.,t».;;;v:•,:., .. ......... :. .4 <br /> sk'"r TPH-Diesel EPA8015M/DHS 1 mg/Kg ND 1 17-Jun-99 ND 50 94.0% 50 86.00/0 84.0% 0.6% <br /> Benzene EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 84.0% 5 80.00/6 82.0°h 0.6% <br /> :................................................................................m::::::::v::::::::n•:::::::::n................................................� ;•::::::.v:.v::;.........................:.......................:......................................... ...........� •................................................................................ .•...........................n......................n..........::.:::::::::::::::::::::::•:.•:::r:::::::nw:::::::v:::.w:::::::::::.:v:::::::::::::;n,•::::::::::::nx„vri <br /> '•: <br /> Toluene EPA 8020 5 ug/Kg ND 1 ` 17-Jun-99 ND 5 98.00/0 5 98.0% 102.0% 1.00,6 <br /> .`•Eth Iben ene v:::::.......:...:::•::::::::..........:::::•:::::.....,.:::::..:.,•:•„•:; <br /> r y z EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 102.0% 5 80.0%' 92.0% 3.5% <br /> ':Xylenes,Total EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 10 92.0% 10 91.0°/0 90.00/0 0.3% <br /> ;Methyl-t-Butyl Ether(MtBE) EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 92.0% 5 84.0% 86.0% 0.6°t6 <br /> mg,1L.=milligrams per Liter=ppm DLR-Detection Linrit•lbr the Purpose oJ• RSD-represent relative percent different(RPD)between duplicates spike ofsanrples <br /> ug/l,=micrograms per Liter=ppb Reporting. lixceptiwial sample matrices ot• or Duplicate ofsample <br /> lv interfereneces nrav result in higher detection <br /> s USAf&D-measure o the percent recover efficiencies within the matrix <br /> C=Composite G=Grab limits f p y <br /> • LCS-measure o(the percent recovery ofthe Laboratory Control Spike(LCS) <br /> ,•-�, RESPE TFULLY UB ITTED, <br /> Jonathan Hao V. Le, Laboratory Director <br /> �', EPet-Iinvirormrenlall'rotectionAgenc}�Llelho�L Page 1 of 1 <br /> ry SblStandard�fethodforLxaminalion ��e€x�rQ���I ,�dSt. Suite A Stockton, CA 95204 Tel.: (209) 462-0892 Fax: (209) 462-7935 <br />