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• • Pace Analytical Services,Inc. <br /> ® 2795 Second Street-Suite 300 <br /> ace Analytical Davis,CA 95618 <br /> ,mxpacelabsc= (530)297-0800 <br /> ANALYTICAL RESULTS <br /> Project: DIESEL LINE SAMPLING <br /> Pace Project No.: 1246740 <br /> Sample: SS-1-DIS@2' Lab ID: 1246740001 Collected: 05/07/15 09:30 Received: 05/07/15 12:30 Matrix: Solid <br /> Results reported on a"wet weight"basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 6010 MET ICP Analytical Method:EPA 60108 Preparation Method:EPA 3050 <br /> Lead 7.9 mg/kg 0.49 1 05/11/1508:00 05112/1509:51 7439-92-1 <br /> 8015 GCS THC-Diesel Analytical Method:EPA 80158 Preparation Method:89 CA LUFT <br /> TPH-DRO(Cl 0-C28) 264 mg/kg 0.99 1 05/12/1516:08 05112/1520:38 DK <br /> Surrogates <br /> n-Octacosane(S) 117 %. 70-130 1 05/1211516:08 05112/1520:38 630-02-4 <br /> Analytical Method:EPA 8260B Preparation Method:EPA 5035/50308 <br /> tert-Amylmethyl ether ND mg/kg 0.25 1 05/13115 13:32 05/13/15 14:53 994-05-8 <br /> Benzene ND mg/kg 0.25 1 05/13/1513:32 05/1311514:53 71-03-2 <br /> tert-Butyl Alcohol ND mg/kg 0.25 1 05/13/1513:32 05113/1514:53 75-65-0 <br /> Diisopropyl ether ND mg/kg 0.25 1 05/13/15 13:32 05113/1514:53 108-20-3 <br /> Ethylbenzene ND mg/kg 0.25 1 05/1311513:32 05/13/1514:53 10041-4 <br /> Ethyl-tert-butyl ether ND mg/kg 0.25 1 05/13115 13:32 05/13/15 14:53 637-92-3 <br /> Methyl-terl-butyl ether ND mg/kg 0.25 1 05/13/15 13:32 05/13/15 14:53 1634044 <br /> Toluene ND mg/kg 0.25 1 05/13/1513:32 0511311514:53 108-88-3 <br /> TPH as Gas ND mg/kg 49.9 1 05/13/15 13:32 05113/1514:53 <br /> Xylene(Total) ND mg/kg 0.50 1 05/13/15 13:32 05113/1514:53 1330-20-7 <br /> Surrogates <br /> 1,2-Dichloroethane-d4(S) 95 %. 70-130 1 05/13115 13:32 05/13/15 14:53 17060-07-0 <br /> Toluene-d8(S) 101 %. 70-130 1 05/1311513:32 05/13/15 14:53 2037-26-5 <br /> 4-Bromofluorobenzene(S) 95 %. 70-130 1 05113/1513:32 05/13115 14:53 460-00-0 <br /> Sample: SS-2110'@2' Lab ID: 1246740002 Collected: 05107/1509:40 Received: 05/07/1512:30 Maldx: Solid <br /> Results reported on a"wet-weight"basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 6010 MET ICP Analytical Method:EPA 6010B Preparation Method:EPA 3050 <br /> Lead 11.0 mg/kg 0.48 1 05/11/1508:00 05/1211509:55 7439-92-1 <br /> 8015 GCS THC-Diesel Analytical Method:EPA 80158 Preparation Method:89 CA LUFT <br /> TPH-DRO(Cl 0-C28) 11.0 mg/kg 0.99 1 05/1211516:08 05/12/1520:03 <br /> Surrogates <br /> n-Octaoosane(S) 129 %. 70-130 1 05/12/1516:08 05112115 20:03 630-02-4 <br /> 8260 MSV UST Analytical Method:EPA 82606 Preparation Method:EPA 5030 Low <br /> tert-Amylmethyl ether ND mg/kg 0.0050 1 05/1111519:44 05/12115 00:44 994-05-8 <br /> Benzene ND mg/kg 0.0050 1 05/11115 19:44 05112/15 00:44 71143-2 <br /> tert-Butyl Alcohol ND mg/kg 0.0050 1 05/11/1519:44 05/12/1500:44 75-65-0 <br /> Diisopropyl ether ND mg/kg 0.0050 1 05/11/1519:44 05/1211500:44 108-20-3 <br /> Ethylbenzene ND mg/kg 0.0050 1 05/11115 19:44 05/12115 00:44 100-41-4 <br /> Ethyl-tert-butyl ether ND mg/kg 0.0050 1 05/11/15 19:44 05112/15 00:44 637-92-3 <br /> Methyl-tert-butyl ether ND mg/kg 0.0050 1 05/11/1519:44 05/12/1500:44 1634-04-0 <br /> Toluene ND mg/kg 0.0050 1 05/11/1519:44 05!1211500:44 108-88-3 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Dale:05/14/2015 07:20 PM without the written consent of PaceAnalytical Services,Inc.. Page 6 of 17 <br />