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• • Pace Analytical Services,Inc. <br /> 02795 Second Street-Suite 300 <br /> aceAnalytical Davis,CA 95618 <br /> w wpacelabicom (530)297A800 <br /> ANALYTICAL RESULTS <br /> Project: DIESEL LINE SAMPLING <br /> Pace Project No.: 1246740 <br /> Sample: SS-2110'@2' Lab ID: 1246740002 Collected: 05/07/15 09:40 Received: 05/07/15 12:30 Matrix: Solid <br /> Results reported on a"wet-weight"basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 8260 MSV UST Analytical Method:EPA 82608 Preparation Method:EPA 5030 Low <br /> TPH as Gas ND mg/kg 0.99 1 05/11/15 19:44 05/12/15 00:44 <br /> Xylene(Total) ND mg/kg 0.0099 1 05/11/1519:44 05/1211500:44 1330-20-7 <br /> Surrogates <br /> 1,2-Dichloroethaned4(S) 96 °h. 70-130 1 05/11/1519:44 05112/1500:44 17060-07-0 <br /> Toluene-d8(S) 100 °h. 70-130 1 05111/15 19:44 05/12115 00:44 2037-26-5 <br /> 4-Bromofluorobenzene(S) 97 %. 70-130 1 05/1111519:44 05/12/1500:44 460-00-4 <br /> Sample: SS-3120'@3' Lab ID: 1246740003 Collected: 05107/15 09:50 Received: 05/07/15 12:30 Matrix: Solid <br /> Results reported on a"wet-weight"basis <br /> Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual <br /> 6010 MET ICP Analytical Method:EPA 6010B Preparation Method:EPA 3050 <br /> Lead 10.6 mg/kg 0.50 1 05/11115 08:00 05/12/15 09:59 7439-92-1 <br /> 8015 GCS THC-Diesel Analytical Method:EPA 8015B Preparation Method:89 CA LUFT <br /> TPH-DRO(C10-C28) 7.7 mg/kg 0.99 1 05/12115 16:08 05112115 18:20 DM <br /> Surrogates <br /> n-Octacosane(S) 90 %. 70-130 1 05/12/15 16:08 05/12/1518:20 630-02-0 <br /> 8260 MSV UST Analytical Method:EPA 8260B Preparation Method:EPA 5030 Low <br /> tert-Amylmethyl ether ND mg/kg 0.0050 1 05/11/1519:44 05/12/1501:07 994-05-8 <br /> Benzene ND mg/kg 0.0050 1 05/11/15 19:44 05112115 01:07 71-43-2 <br /> tert-Butyl Alcohol ND mg/kg 0.0050 1 05/1111519:44 05112/1501:07 75£5-0 <br /> Diisopropyl ether ND mg/kg 0.0050 1 05/1111519:44 05/1211501:07 108-20-3 <br /> Ethylbenzene ND mg/kg 0.0050 1 05/1111519:44 05/12/1501:07 10041-4 <br /> Ethyl-tert-butyl ether ND mg/kg 0.0050 1 05/11/15 19:44 05/12/15 01:07 637-92-3 <br /> Methyl-tert-butyl ether ND mglkg 0.0050 1 05/11/15 19:44 05112/15 01:07 163404A <br /> Toluene ND mglkg 0.0050 1 05/11/1519:44 0511211501:07 108-88-3 <br /> TPH as Gas ND mg/kg 0.99 1 0511111519:44 05/12115 01:07 <br /> Xylene(Total) ND mg/kg 0.0099 1 05/1111519:44 05/1211501:07 1330-20-7 <br /> Surrogates <br /> 1,2-Dichloroethaned4(S) 98 %. 70130 1 05/11/1519:44 05/1211501:07 17060-07-0 <br /> Toluene c18(S) 101 %. 70-130 1 05/11/15 19:44 05112115 01:07 2037-26-5 <br /> 4-Bromofluorobenzene(S) 98 %. 70-130 1 05/11/1519:44 05/12/1501:07 460-00-0 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:05114/2015 07:20 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 17 <br />