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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell corn <br /> tAdvanced GeoEnvironmental Client Project ID Chet's Auto Date Sampled 10123-24/01 <br /> 837 Shaw Road Date Received 10/25/01 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 10/25/01 <br /> Client P O Date Analyzed 10130-10/31/01 <br /> ' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 81995 <br /> ' Client ID 131-10' <br /> Matrix S <br /> Compound Concentration* Reporting Limit * Rcponmg Linut <br /> p W g Compound Concentration <br /> 1 W S <br /> Acetone tn1 ND<26,000 5 0 25 trans-l,3-DtchloropioQene ND<2500 1 0 so � <br /> Benzene ND<2500 to 50 Ethylene dibromide ND<2500 1 0 50 <br /> Bromobenzene ND<2500 l 0 50 Ethyibenzene 44,000 1 0 50 <br /> ' Bromochloromethane ND<2500 l 0 50 Hexachlorobutadiene ND<12500 50 25 <br /> BromodichIoromethane ND<2500 10 50 lodomethane ND<2500 1 0 50 <br /> Bromoform ND<2500 1 0 1 50 Isopropylbenzene 8100 1 0 50 <br /> Bromomethane ND<2500 1 0 5 0 p-Isopropyl toluene ND<2500 1 0 5 0 <br /> n-Butyl benzene 20,000 10 5 0 Methyl butyl ketone 1 ND<2500 1 0 50 <br /> sec-Butyl benzene ND<2500 10 5 0 Methylene Chlonde° ND<2500 10 5 0 <br /> tert-Butyl benzene ND<2500 10 5 0 Methyl ethyl ketone ND<5000 2 0 10 <br /> Carbon Disulfide ND<2500 10 5 0 Methyl isobutyl ketones N13<2500 1 0 5 0 <br /> Carbon Tetrachloride ND<2500 10 5 0 Methyl Cert-Butyl Ether(MTBE) -- 1 0 5 0 <br /> Chlorobenzene ND<2500 10 5 0 Naphthalene 24,000 5 0 50 <br /> Chloroethane ND<2500 10 50 n-Propyl benzene 32,000 1 0 50 <br /> 2-Chloroethyl Vinyl Ether"' ND<2500 1 0 11 Styrene ND<2500 1 0 50 <br /> Chloroform ND<2500 10 5 0 1,1,1,2-Tetrachloroethane ND<2500 1 0 5 0 <br /> Chloromethane ND<2500 to 5 0 1,1,2,2-Tetrachloroethane ND<2500 1 0 5 0 <br /> 2 Chlorotoluene ND<2500 1 0 50 Tetrachloroethene ND<2500 1 0 5 0 <br /> 4-Chlorotoluene ND<2500 l 0 5 0 Toluene 31,000 1 0 5 0 <br /> Dibromochloromethane ND<2500 1 0 5 0 1,2,3-Tnchlombenzene ND<12500 5 0 25 <br /> 1,2-Dibromo-3-chlompropane ND<5000 2 0 10 1,2,4-Tnchlombenzene ND<12500 50 25 <br /> Dibromomethane ND<2500 1 0 5 0 1,1,1-Tnchloroethane ND<25W to 50 <br /> 1,2-Dichlorobenzene ND<2500 10 50 1,t,2-Tnchlomethane ND<2500 10 50 <br /> 1,3-Dichiorobenzene ND<2500 1 0 5 0 Trichloroethene ND<2500 1 0 50 <br /> 1,4-Dichlorobenzene ND<2500 1 0 5 0 Trichlorofluoromethane ND<2500 10 50 <br /> Dichlorodifluoromethane ND<2500 1 0 5 0 1,2,3-Tnchloropropane ND<2500 1 0 5 0 <br /> t,]-Dichlomethane ND<2500 1 0 5 0 1,2,4-Trimethylbenzene 190,000 10 5 0 <br /> t,2-Dichloroethane ND<2500 10 5 0 1,3,5-Tnmethylbenzene 67,000 10 5 0 <br /> IJ-Dichloroethene ND<2500 10 5 0 Vinyl Acetate ND<12500 50 25 <br /> cis-1,2-Dichloroethene ND<2500 10 50 Vinyl Chloride ° ND<2500 10 50 <br /> 1 trans-ll Dichloroethene ND<2500 10 5 0 Xylenes,total ° 300,000 1 0 50 <br /> 1,2-Dichloropropane ND<2500 1 0 5 0 Comments <br /> t,3-Dichtoropmpane ND<2500 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<2500 10 5 0 Dibromofluoromethane 97 <br /> 1,1-Dichloropropene ND<2500 10 50 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<2500 1 0 5 0 4-Bromotluorobenzene 107 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples i ug/kg, ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not ap le to this analysts <br /> ' (b) 2-propanone or dimethyl ketone, (c)(2-c1loroethoxy) ethene, ld) 2-hexanonc, (e) dichloromethane 11 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen is present. (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> ' chioroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />