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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//ww%vmcr-jTpbe1lccm E-mail main@mccampbell com <br /> Advanced GeoEnvirontnental Client Project ID Chet's Auto Date Sampled 10/23-24/01 <br /> 837 Shaw Road Date Received 10/25/01 <br /> Stockton,CA 95215 Client Contact Bill Little Date Extracted 10/25/01 <br /> Client P O Date Analyzed 10/30-10/31/01 <br /> Volatile Organics By GC/MS <br /> EPA method 5260 <br /> Lab ID 81996 <br /> Client ID B1-20' <br /> Matrix S <br /> Compound Concentration* Rep—g Limit Compound Concentration* Rcportmg Limit <br /> S <br /> Acetone c6) ND<2600 50 25 trans-1,3-Dtchioro1propene ND<250 1 fl 50 <br /> Benzene ND<250 10 50 Ethylene dibrom,de ND<250 10 50 <br /> Bromobenzene ND<250 1 0 50 Ethylbenzene 2800 ]q 50 <br /> Bromochloromethane ND<250 1 0 50 Hexachlorobutadiene ND<1250 50 25 <br /> Bromodichloromethane ND<250 10 50 Iodomethane ND<250 10 50 <br /> Bromoform NIX250 10 50 Isopropyibenzene 420 to 50 <br /> Bromomethane ND<250 10 50 p-Isopropyl toluene ND<250 l 0 50 <br /> n-Butyl benzene 860 1 0 50 Methyl butyl ketone ND<250 10 50 <br /> sec-Butyl benzene ND<250 l 0 50 Methylene Chloride"' ND<250 1 0 50 <br /> tert-Butyl benzene ND<250 10 50 Methyl ethyl ketone ND<500 2 0 10 <br /> Carbon Disulfide 111)<250 1 0 5 0 Methyl,,.butyl ketone ND<250 1 0 50 <br /> Carbon Tetrachloride ND<250 l 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND<250 10 50 Naphthalene 1300 50 50 <br /> Chloroethane ND<250 10 50 n-Propyl benzene 1800 10 50 <br /> 2-Chloroethyl Vinyl Eth ND<250 10 5 0 Styrene ND<250 10 50 <br /> Chloroform ND<250 10 50 1,1,1,2-Tetrachloroethane ND<250 10 50 <br /> Chloromethane ND<250 10 50 1,1,2 2-Tetrachloroethane ND<250 1 0 50 <br /> 2-Chlorotoluene ND<250 10 50 Tetrachloroethene ND<250 1 0 50 <br /> ' 4-Chlorotoluene ND<250 10 50 Toluene 1400 1 0 50 <br /> D,bromochloromethane ND<250 10 50 1,2,3-Tnchlorobenzene ND<1250 50 25 <br /> 1,2-Dibromo-3-chloropropane ND<500 20 10 1,2,4-Tnchlorobenzene ND<1250 50 25 <br /> Dibromomethane ND<250 10 50 1,1,1-Trichloroethane ND<250 10 50 <br /> 1 1,2-Dichlorobenzene ND<250 10 50 1,1,2-Tnchloroethane ND<250 to 50 <br /> 1,3-Dichlorobenzene ND<250 1 0 50 Trichloroethene ND<250 1 0 50 <br /> 1,4-Dichlorobenzene ND<250 10 50 Trichlorofluoromethane ND<250 10 50 <br /> Dichlorodifluoromethane ND<250 10 50 1,2,3-Trichloropropane ND<250 1 0 50 <br /> ' 1,1-Dichloroethane ND<250 10 50 1,2,4-Tnmethylbenzene 8200 10 50 <br /> 1,2-Dtchloroethane ND<250 l0 50 1,3,5-Trimethylbenzene 2600 10 50 <br /> 1,1-Dtchloroethene ND<250 10 50 Vinyl Acetate ') ND<1250 50 25 <br /> cis-1,2-Dtchloroethene ND<250 to 50 Vinyl Chloride ND<250 l 0 50 <br /> 1 trans-1,2 Dichloroethene ND<250 to 50 Xylenes,total ° 17 000 l 0 50 <br /> 1,2-Dichloropropane ND<250 to 50 Comments <br /> I,3-D,chloropropane ND<250 l 0 50 Surrogate Recoveries <br /> 2,2-Dichioropropane ND<250 l 0 50 Dibromotluoromethane 96 <br /> ' 1,1-Dichloropropene ND<250 to 50 Toluene-0 102 <br /> cis-t,3-Dichloropropene ND<250 10 50 4-Bromotluorobenzene 106 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples,n ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlornethoxy) ethene (d) 2-hexanone, (e) dichlommethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (b)lighter than water in nisc,ble sheen is present (t)liquid sample that contains greater than–5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, 3) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> ' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />