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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, 1tvne,CA 92614(949)261-1022 Fm:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Nary Dr., Stockton,CA �� <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IUI1062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit MDL Result Factor Extracted Analyzed Qualifiers <br /> Sample ID: IU11062-13(MW-14-Water) Sampled:09/08/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 8260B 1111489 0.50 0.28 1.7 1 9/14/2011 9/14/2011 <br /> Ethylbenzene EPA 82608 1111489 0.50 0.25 ND 1 9/14/2011 9/14/2011 <br /> Toluene EPA 8260B 1111489 0.50 0.36 0.40 1 9/14/2011 9/14/2011 1 <br /> Xylenes,Total EPA 8260B 1111489 1.0 0.90 ND 1 9/14/2011 9/14/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82606 1111489 1.0 0.25 18 1 9/14/2011 9/14/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111489 1.0 0.32 ND 1 9/14/2011 9/14/2011 <br /> tert-Butanol(TBA) EPA 8260B 1111489 10 6.5 ND 1 9/14/2011 9/14/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 107% <br /> Surrogate: Dibromofluoromethane(80-120%) 109% <br /> Surrogate: Toluene-d8(80420%) 104% <br /> Sample ID:IUII062-14(MW-15-Water) Sampled:09/08/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 8260B 1111489 - 0.50 0.28 1.3 1 9/14/2011 9/14/2011 <br /> Ethylbenzene EPA 82608 1111489 0.50 0.25 0.53 1 9/14/2011 9/14/2011 <br /> Toluene EPA 8260B 1111489 0.50 0.36 2.2 1 9/14/2011 9/14/2011 <br /> Xylenes,Total EPA 82606 1111489 1.0 0.90 4.5 1 9/14/2011 9/14/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111489 1.0 0.25 9.5 1 9/14/2011 9/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 1111489 1.0 0.28 ND 1 9114/2011 9/14/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111489 1.0 0.32 17 1 9/14/2011 9/14/2011 <br /> tert-Butanol(TBA) EPA 8260B 1111489 10 6.5 12 1 9/14/2011 9/14/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 106% <br /> Surrogate:Dibromofluoromethane(80-1200%) 106% <br /> Surrogate: Toluene-d8(80-120%) 105% <br /> Sample ID:IU11062-15(MW-16-Water) Sampled:09/08/11 <br /> Reporting Units: ug/1 <br /> Benzene EPA 82608 1111489 1.0 0.56 380 2 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111489 1.0 0.50 7.2 2 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111489 1.0 0.72 22 2 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 82608 1111489 2.0 1.8 26 2 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111489 2.0 0.50 ND 2 9/14/2011 9/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111489 2.0 0.64 ND 2 9/14/2011 9/15/2011 <br /> tert-Butanol(TBA) EPA 82608 1111489 20 13 ND 2 9/14/2011 9/15/2011 <br /> Surrogate:4-Bromoffuorobertzene(80-12001o) 104% <br /> Surrogate:Dibromofluoromethane(80-120%) 99% <br /> Surrogate: Tofuene-d8(80-120%) 105% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The resutls pertain only to the samples tested in the laboratory. This report shall not be repraduced, <br /> except in full,without written permission from TestAmerica. 1U11062 <Page 19 of 67> <br />