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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fas:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr., Stockton.CA <br /> 1680 Rogers Avenue <br /> Sampled: 09/07/11-09/09/1) <br /> San Jose,CA 95112-1105 <br /> ReportNumber: IUII062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit MDL Result Factor Extracted Analyzed y Qualifiers <br /> Samplefl): IU11062-16(MW-18-Water) Sampled: 09/08/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 82608 11(1489 0.50 0.28 0.91 1 9/14/2011 9/14/2011 <br /> Ethylbenzene EPA 82608 1111489 0.50 0.25 ND 1 9/14/2011 9/14/2011 <br /> Toluene EPA 8260B 1111489 0.50 0.36 ND 1 9/14/2011 9/14/2011 <br /> Xylenes,Total EPA 82608 <br /> 1111489 1.0 0.90 ND I 9/14/2011 9/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 1111489 1.0 0.25 9.7 1 9/14/2011 9/14/2011 <br /> tert-Butanol(TBA) EPA 82608 1111489 10 6.5 56 1 9/14/2011 9/14/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 102% <br /> Surrogate. Dibromofluoromethane(80-120%) 102% <br /> Surrogate: Toluene-d8(80-120%) 104 <br /> Sample ID: IUI1062-17(MW-19-Water) Sampled:09/08/11 <br /> Reporting Units: ugn <br /> Benzene EPA 82608 1111489 0.50 0.28 6.1 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111489 0.50 0.25 0.26 1 9/14/2011 9/15/2011 J <br /> Toluene EPA 8260B 1111489 0.50 0.36 ND 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 1111489 IA 0.90 ND 1 9/14/2011 9/15/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-110916) 100% <br /> Surrogate:Dibromofluoromethane(80-120%) 106% <br /> Surrogate: Toluene-d8(80-120%) 105% <br /> Sample ID: IUI1062-I8(MW-20-Water) Sampled: 09/09/11 <br /> Reporting Units: ug/l <br /> Benzene EPA 82608 1112257 5.0 2.8 140 10 9/20/2011 9/20/2011 <br /> Ethylbenzene EPA 82608 <br /> 1112257 5.0 2.5 ND 10 9/20/2011 9/20/2011 <br /> 'Toluene EPA 82608 1112257 5.0 3.6 13 10 9/20/2011 9/20/2011 <br /> Xylenes,Total EPA 8260B 1112257 10 9.0 27 <br /> 10 9/20/2011 9/20/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1112257 10 2.5 4.0 10 9/20/2011 9/20/2011 <br /> Ethyl tert-Butyl Ether(ETBE EPA 82608 J <br /> ) III2257 10 2.8 2.9 10 9/20/2011 9/20/2011 1 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1112257 10 3.2 120 10 9/20/2011 9/20/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 1112257 10 3.3 ND 10 9/20/2011 9/20/2011 <br /> tert-Butanol(TBA) EPA 8260B 1112257 100 65 6600 10 9/20/2011 9/20/2011 <br /> Surrogate:4-Bromofluorobenzene(80-110%) 105% <br /> Surrogate:Dibromofluoromethane(80-120916) 101 % <br /> Surrogate: Toluene-d8(80-120%) 107% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except m full,without written permission from TestAmerica. 71111061 <Page 10 of 67> <br />