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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Nary Dr,Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose.CA 95112.1105 ReportNumber: IU11062 Received: 09/13/11 <br /> Attention: Lorin King <br /> METHOD BLANK/QC DATA <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch: 1112257 Extracted:09/20/11 <br /> Matrix Spike Analyzed:09/20/2011 (1112257-MSI) Source: IU11608-03 <br /> Benzene 26.3 0.50 ug/I 25.0 ND 105 65-125 <br /> Ethylbenzene 31.3 0.50 ug/I 25.0 ND 125 65-130 <br /> Toluene 29.1 0.50 ugA 25.0 ND 116 70-125 <br /> m,p-Xylenes 62.0 1.0 ug/I 50.0 ND 124 65-130 <br /> o-Xylene 30.5 0.50 ug/I 25.0 ND 122 65-125 <br /> Xylenes,Total 92.5 1.0 ugA 75.0 ND 123 60-130 <br /> Di-isopropyl Ether(DIPE) 27.0 1.0 ug/I 25.0 ND 108 60-140 <br /> Ethyl tert-Butyl Ether(ETBE) 30.2 1.0 ug/I 25.0 ND 121 60-135 <br /> Methyl-tert-butyl Ether(MTBE) 29.7 1.0 ug/I 25.0 1.86 1 I 1 55-145 <br /> tert-Amyl Methyl Ether(TAME) 30.2 1.0 ug/1 25.0 ND 121 60-140 <br /> tert-Butanol(TBA) 155 10 ug/I 125 ND 124 65-140 <br /> Surrogate:4-Bromofluorobemene 26.8 u9/1 25.0 107 80-129 <br /> Surrogate:Dibromoflucromethane 15.6 ug/1 25.0 102 80-120 <br /> Surrogate:Toluene-d8 27.2 119/1 25.0 109 80-120 <br /> Matrix Spike Dup Analyzed:09/20/2011 (1112257-MSDI) Source:IU11608-03 <br /> Benzene 27.6 0.50 ug/I 25.0 ND Ill 65-125 5 20 <br /> Ethylbenzene 31.6 0.50 ugA 25.0 ND 127 65-130 1 20 <br /> Toluene 30.3 0.50 ugA 25.0 ND 121 70-125 4 20 <br /> m,p-Xylenes 63.3 1.0 ug/I 50.0 ND 127 65-130 2 25 <br /> o-Xylene 31.2 0.50 ug0 25.0 ND 125 65-125 2 20 <br /> Xylenes,Total 94.5 1.0 ugA 75.0 ND 126 60-130 2 20 <br /> Di-isopropyl Ether(DIPE) 28.6 1.0 ugA 25.0 ND 114 60-140 5 25 <br /> Ethyl tert-Butyl Ether(ETBE) 32.4 1.0 ugA 25.0 ND 130 60-135 7 25 <br /> Methyl-tert-butyl Ether(MTBE) 32.1 1.0 ugA 25.0 1.86 121 55-145 8 25 <br /> tert-Amyl Methyl Ether(TAME) 33.2 1.0 ug/I 25.0 ND 133 60-140 10 30 <br /> ted-Butanol(TBA) 143 10 ugA 125 ND 114 65-140 8 25 <br /> Surrogate:4-Bromofluorobenzene 26.5 ug/I 25.0 106 80-120 <br /> Surrogate:Dibromofluoromethane 26.0 119/1 25.0 104 80-120 <br /> Surrogate:Toluene-d8 27.4 u9/7 25.0 109 80-110 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except m full,without written permission from TestAmerica 1 U11061 <page 65 of 67> <br />