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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, lNine,CA 92614(949)261-1022 Fm:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr., Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 ReportNumber: IUI1062 Received: 09/13/11 <br /> Attention: Lorin King <br /> DATA QUALIFIERS AND DEFINITIONS <br /> J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. <br /> M2 The MS and/or MSD were below the acceptance limits due to sample matrix interference. See Blank Spike(LCS). <br /> MNRI There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike/Blank Spike <br /> Duplicate. <br /> P-HS Sample container contained headspace. <br /> QPl Hydrocarbon result partly due to individual peak(s)in quantitation range. <br /> Z Due to sample matrix effects,the surrogate recovery was below the acceptance limits. <br /> Z3 The sample required a dilution due to the nature of the sample matrix. Because of this dilution,the surrogate spike <br /> concentration in the sample was reduced to a level where the recovery calculation does not provide useful <br /> information. <br /> NO Analyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified. <br /> RPD Relative Percent Difference <br /> ADDITIONAL COMMENTS <br /> For 9260 analyses: <br /> Due to the high water solubility of alcohols and ketones,the calibration criteria for these compounds is<30%RSD. <br /> The average%RSD of all compounds in the calibration is 15%, in accordance with EPA methods. <br /> For Volatile Fuel Hydrocarbons(C4-02): <br /> Volatile Fuel Hydrocarbons(C4-C12)are quantitated against a gasoline standard. Quantitation begins immediately before TBA-d9. <br /> For Extractable Fuel Hydrocarbons(EFH,DRO,ORO): <br /> Unless otherwise noted,Extractable Fuel Hydrocarbons(EFH,DRO,ORO)are quantitated against a Diesel Fuel Standard. <br /> TestAtnerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples rested in the laboratory. This repos.shall not be reproduced, <br /> except injull,without written permission from TestAmerica. IU11062 <Page 66 oj67> <br />