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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTINC 17461 Damn Avenue.Suite 100, 1,ine,CA 92614(949)261-1032 Pax.(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-17(AS-]0-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82606 11D]531 0.0010 0.0018 0.996 4/13/2011 4/14/2011 <br /> Ethylbenzene EPA 8260B IID1531 0.0010 0.010 0.996 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B IIDI 531 0.0010 ND 0.996 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260B 11D1531 0.0020 0.050 0.996 4/13/2011 4/14/2011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B 11DI531 0.0020 ND 0.996 4/13/2011 4/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 1IDIS31 0.0020 ND 0.996 4/13/2011 4/14/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B l ID1531 0.0020 0.0052 0.996 4/13/2011 4/14/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B I IDI 531 0.0020 ND 0.996 4/13/2011 4/14/2011 <br /> tert-Butanol(TBA) EPA 82608 I ID 1531 0.020 ND 0.996 4/13/2011 4/14/2011 <br /> Surrogate:4-Bromofluorobenzene(80-120916) 94% <br /> Surrogate:Dibromoj(uoromethane(80-125%) 102% <br /> Surrogate:Toluene-0(80-120%) 101% <br /> Sample ID:IUD0863-18(AS-]0-]0-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D1531 0.0053 0.11 5.32 4/132011 4/14/2011 <br /> Ethylbenzene EPA 82606 IID1531 0.0053 0.17 5.32 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B 11D1531 0.0053 ND 5.32 4/132011 4/14/2011 <br /> Xylenes,Total EPA 8260B IID1531 0.011 0.012 5.32 4/132011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11DI531 0.011 ND 5.32 4/132011 4/142011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D1531 0.011 ND 5.32 4/132011 4/14/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82606 11D1531 0.011 0.66 5.32 4/132011 4/14/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B I ID1531 0.011 ND 5.32 4/132011 4/14/2011 <br /> Cert-Butanol(TBA) EPA 8260B 11D1531 0.11 0.18 5.32 4/13/2011 4/14/2011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 100% <br /> Surrogate:Dibromofluoromethane(80-125%) 102% <br /> Surrogate.' Toluene-&(80-12091) 106% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results Perkin only to the samples rested in the laboratory. This report shall not be reproduced, <br /> exceptinfull,withounerlaenpennisstonfrom TestAmerica. IUD0863 apage13o,(37> <br />