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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Depen Avenue.suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 ReportNumber: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-21(AS-13-5-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82608 11D1531 0.0010 0.026 1.01 4/13/2011 4/14/2011 <br /> Ethylbenzene EPA 8260E 11131531 0.0010 0.050 1.01 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B 11D1531 0.0010 0.0018 1.01 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260B 11D1531 0.0020 0.19 1.01 4/132011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 11D1531 0.0020 NO 1.01 4/132011 4/142011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260E 1ID1531 0.0020 ND 1.01 4/132011 4/142011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11DI531 0.0020 0.0021 1.01 4/13/2011 4/142011 <br /> ten-Amyl Methyl Ether(TAME) EPA 8260B 11D1531 0.0020 ND 1.01 4/132011 4/142011 <br /> tert-Butanol(TBA) EPA 82608 11131531 0.020 0.031 1.01 4/132011 4/142011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 105% <br /> Surrogate:Dibromofluoromethane(80-125%) 107016 <br /> Surrogate: Toluene-0(80-120%) 106% <br /> Sample ID:100863-22(AS-13-10-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D1513 0.049 0.25 97.8 4/132011 4/142011 <br /> Ethylbenzene EPA 8260B 11D1513 0.049 0.79 97.8 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B 11D1513 0.049 ND 97.8 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260E 11D1513 0.098 2.0 97.8 4/13/2011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D1513 0.098 ND 97.8 4/132011 4/142011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D1513 0.098 ND 97.8 4/132011 4/142011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 11D1513 0.098 NO 97.8 4/132011 4/14/2011 <br /> ten-Amyl Methyl Ether(TAME) EPA 82608 11D1513 0.098 ND 97.8 4/13/2011 4/142011 <br /> tert-Butanol(TBA) EPA 8260B 11D1513 0.98 ND 97.8 4/132011 4/142011 <br /> Surrogate:4-Bromofluorobenzene(65-140%) 105% <br /> Surrogate:Dibromofluoromethane(55-140%) 101% <br /> Surrogate: Toluene-d8(60-140916) 104% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. TMs report shall not be reproduced, <br /> except infill,without writtenpermisslonfrom TestAmerica. 1UD0863 <Page14Of37> <br />