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i 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> 4 MCCAMPBELL ANALYTICAL INC. Telephone:510-798-1620 Fax:510-798-1622 <br /> httl):HwwNv.mccampbell.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Steel Guard Date Sampled:08/18/97 <br /> 1803 West March Lane,Ste A Date Received:08/20/97 <br /> Stockton,CA 95207 Client Contact:Bill Little Date Extracted: 08/20/97 <br /> Client P.O: Date Analyzed:08/20-08/22/97 <br /> Volatile Organics By GC/AIS <br /> EPA method 624 or 8240 <br /> Lab ID 79957 <br /> Client ID P3-5 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone(b) ND<200 cis-1,3-Dichloropropene ND<200 <br /> Benzene ND<200 trans-1,3-Dichloropropene ND<200 <br /> Bromodichloromethane ND<200 Ethylbenzene 240 <br /> Bromoform ND<200 Methyl butyl ketone(d) 14D<200 <br /> Bromomethane ND<200 Methylene Chloride(') ND<200 <br /> Carbon Disulfide ND<200 Methyl ethyl ketone(0 ND<200 <br /> Carbon Tetrachloride ND<200 Methyl isobutyl ketone ND<200 <br /> Chlorobenzene ND<200 Styrene(k) ND<200 <br /> Chloroethane ND<200 1,1,2,2-Tetrachloroethane ND<200 <br /> 2-Chloroethyl Vinyl Ether(`) ND<200 Tetrachloroethene ND<200 <br /> Chloroform ND<200 Toluene(') ND<200 <br /> Chloromethane ND<200 1,1,1-Trichloroethane ND<200 <br /> Dibromochloromethane ND<200 1,1,2-Trichloroethane ND<200 <br /> 1,2-Dichlorobenzene ND<200 Trichloroethene ND<200 <br /> 1,3-Dichlorobenzene ND<200 Trichlorofluoromethane ND<200 <br /> 1,4-Dichlorobenzene ND<200 Vinyl Acetate(m) ND<200 <br /> 1,1-Dichloroethane ND<200 Vinyl Chloride(n) ND<200 <br /> 1,2-Dichloroethane ND<200 Xylenes,total (o) (15 00 <br /> 1,1-Dichloroethene ND<200 Surrogate Recoveries(`%) <br /> cis-1,2-Dichloroethene ND<200 Dibromofluoromethane 101 <br /> trans-1,2-Dichloroethene ND<200 Toluene-d8 98 <br /> 1,2-Dichloropropane ND<200 4-Bromofluorobenzene 87 <br /> Comments: <br /> -water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP!SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy)ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. CN <br /> DHS Certification No. 1644 Ce- Edward Hamilton,Lab Director <br />