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110 Second Avenue South,##D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone:510-798-1620 Fax:510-798-1622 <br /> http://www.mccanipbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Steel Guard Date Sampled:08/18/97 <br /> 1803 West March Lane,Ste A Date Received:08/20/97 <br /> Stockton,CA 95207 Client Contact:Bill Little Date Extracted:08/20/97 <br /> Client P.O: Date Analyzed:08/20-08/22/97 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 79957 <br /> Reporting Limit <br /> Client ID P3-5 <br /> Matrix S W <br /> Compound Concentration* ug-1 g u<iL <br /> Di-isopropyl Ether(DIPE) ND<50 5.0 1.0 <br /> Ethanol ND<1000 100 20 <br /> Ethyl tert-Butyl Ether(ETBE) ND<50 5.0 1.0 <br /> Methanol --- --- --- --- N/A N/A <br /> Methyl-tert Butyl Ether(MTBE) ND<50 50 5.0 <br /> tert-Amyl Methyl Ether(TAME) ND<50 5.0 1.0 <br /> tert-Butanol ND<250 25 5.0 <br /> Surrogate Recoveries('%.) <br /> Dibromofluoromethane 101 <br /> Toluene-d8 98 <br /> Comments: i F__1=1 <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />