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Associated Laboratories <br /> QA / QC EPA Methods 8260, 624, & 524.2 - GCMS # 3 <br /> Sample ID: MS/MSD-water sample 155931-702 <br /> Date Analyzed September 1 , 2005 4 47pm <br /> Sample Matrix: water <br /> Units: pg/L <br /> Applies to LR- 155934, 155931, 155964, 155980 <br /> Sample I Spike Spike Oup S Ike Dup QC Limits <br /> IlCompound Cone. Added Res Res % Rea % Roe RPD RPD % Rae <br /> 1,1-Dichloroethene 000 500 4829 4736 97 95 2 22 59 - 172 <br /> MTBE 14811 500 201.65 20414 107 112 5 24 62 - 137 <br /> Benzene 000 500 56 92 55 56 1 114 111 2 24 62 - 137 <br /> Trichloroethene 000 500 51 94 5096104 102 2 21 66 - 142 <br /> Toluene 000 500 5332 53 01 107 106 1 21 59 - 139 <br /> Chlorobenzene 000 500 51 51 5287 103 106 3 21 60 - 133 <br /> Sample ID: LCS - water <br /> Date Analyzed. September 1 , 2005 12:37pm <br /> Sample Matrix- water <br /> Units: pg/L <br /> Sam le Spike Spike Spike QC Limits <br /> Compound Cork. Added Res % Roe RPD % Roe <br /> 1,1-Dichloroethene 000 500 47 63 95 22 59 - 172 <br /> MTBE 000 500 5294 106 24 62 - 137 <br /> Benzene 000 500 51 96 104 1 24 62 - 137 <br /> Trichloroethene 000 500 4945 99 21 166 - 142 <br /> Toluene 000 500 5223 104 21 59' - 139 <br /> Chlorobenzene 000 50.0 51 96 104 21 60 - 133 <br /> Surrogate Recovery GCMS # 3 <br /> Limits <br /> Compound MBI M02 MS MSD LCS % Rea <br /> Dibromofluoromethane 99 103 89 92 88 70-135 <br /> 1,2-Dichloroethane-d4 111 110 93 89 89 70-135 <br /> Toluene-d8 103 96 102 1 99 95 1 11 70-135 <br /> p-Bromofluorobenzene 100 1 99 1 88 9j_1 92 170-135 <br /> 8260LB_09 <br />