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ASSOCIATED LABORATORIES <br />--- --- --- -- - --�- - C EPA-Methods-8260,-624,-&-52-4.2_ __GCMS# 3, <br /> Sample ID. MS/MSD-water sample 155934-735 <br /> Date Analyzed. August 31,, 2005 12:25am <br /> Sample Matrix* water <br /> Units: pg/L <br /> Applies to LR- 155934 <br /> Sample Spike Spike Dup Spike Dup QC Limits <br /> Compound Cone Added, Res Res % Roe % Rea RPD RPD % Roe <br /> 1,1-Dichloroethene 0 00 500 51 98 5032 104 101 3 22159 - 172 <br /> MTBE 0 00 500 6223 6074 124 121 2 24 62 - 13 7 <br />_ - - <br /> Benzene - _ 0 00 500 5833 5898 117 118 1 24 fit - 137 <br /> _ 0 00 50 0 52 99 49 31 106 99 7 T 21- 66`- 142 <br /> Trichloroethene - <br /> Toluena 0 00 50 0 53 67 51 68 107 103 4 21 59 - 139 <br /> 139 <br /> Chlorobenzene 0 00 11 <br /> 00 5257 524 105 105 0 21 60 - 133 <br /> Sample ID: LCS - water - - <br /> Date Analyzed ,August 31 , 2005 8:27am i <br /> Sample Matrix- water <br /> Units pg/L <br /> Sample Spike Spike" -Spike-- —_ - - - = QC F_ —Limits.-T <br /> =Cont = -Added= --.--Res— �__ % Rec RPD % Rec <br /> --- - WFCLJ,1_7=Dich1oroethene <br /> nd- - ---= - - <br /> 22 59 -_02 <br /> 0 00 50 0 52 38 1 O5 - 24 62 137 <br /> MTBE 000 .500 6.075 m _ 121 ^L <br /> Benzene <br /> 000 500 5775 115 24 62 - 137 <br /> 21 66 - 142 <br /> Trichloroethene 000 50 0 5368 107 21 59 - 139 <br /> Toluene 000 500 51 96 104 <br /> Chlorobenzene <br /> 000 500 51 78 104 21 60 - 133 <br /> Surrogate Recovery GGMS # 3 <br /> Limits <br /> Mgt MS MSD LCS % Rec <br /> C <br /> ompound 70-135 <br /> 105 100 104 96 <br /> 108 90 91 94 70-135 <br /> 1,2-Dichloroethane-d4 70-135 <br /> Toluene-d8 100 100 99 98 <br /> p-Bromofluorobenzene <br /> gg 95 100 94 70-1 <br /> 8260LB 08 xis <br />