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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample 1D: B4A@5.0-5.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-09 <br /> Site: <br /> Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit ail.Factor QUAL Date Analyzed Analyst Seq.# <br /> DIESEL RANGE ORGANICS MCL CA_DRO Units:mg/Kg <br /> Diesel Range Organics 13 2 1 07/01/04 23:36 AE 2305390 <br /> Surr:n-Pentacosane 97.7 % 20-154 1 07/01/04 23:36 AE 230T39-0— <br /> jPrep Method Pren Date Pre Initials 1PreRFactor <br /> 5W355013 06/29/200413:47 IDMN 1.00 <br /> Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> `-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 20 <br /> 1 7B04 3.'.0624 PM <br />