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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> HOUSTON,TX 77054 <br /> (793)660-0901 <br /> Client Sample ID: 65@2.0-2.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-10 <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> DIESEL RANGE ORGANICS MCL CA DRO Units: mglKg <br /> Diesel Range Organics 7 2 1 07/02/04 0:55 AE 2305392 <br /> Surr: n-Pentacosane 87.5 % 20-154 1 07/02/04 0:55 AE 2305392 <br /> Prep Method Prep Date IPmp Inifials lPrep Factor <br /> SW35508 061291200413:47 DMN 1,00 <br /> MERCURY,TOTAL MCL SW7471A Units: mg/Kg <br /> Mercury ND 0.03 1 07/0310415:04 JAB 2298924 <br /> ' Pre Method Oren Date On Initials Pre Factor <br /> SW7471A 07/02/2004 9:50 JAB 1.00 <br /> METALS BY METHOD 60106,TOTAL MCL SW6010B Units: mg/K <br /> Antimony 6.44 0.5 1 0710310417:29 NS 2299071 <br /> Arsenic 5.85 0.5 1 07103/0417:29 NS 2299071 <br /> Lead 3.96 0.5 1 07/03/04 17:29 NS 2299071 <br /> Selenium ND 0.5 1 0710310417:29 NS 2299071 <br /> Thallium ND 0.5 1 0710310417:29 NS 2299071 <br /> Barium 115 0.5 1 07/02/04 22:39 NW 2298553 <br /> Beryllium ND 0.5 1 07/02/04 22:39 MW 2298553 <br /> Cadmium ND 0.5 1 07/03/04 21.59 MW 2300347 <br /> Chromium 24.5 1 .1 07/02/04 22:39 MW 2298553 <br /> Cobalt 6.4 1 1 07/02/04 22:39 MW 2298553 . <br /> Copper 27.1 1 1 07/02/04 22:39 MW 2298553 <br /> Molybdenum ND 2 1 07/02/04 22:39 MW 2298553 <br /> Nickel 24.7 2 1 07/02/04 22:39 WV 2298553 <br /> Silver ND 1 1 07/02/04 22:39 MW 2298553 <br /> Vanadium 42.5 0.5 1 07/02/04 22:39 MW 2298553 <br /> Zinc 58.9 2 1 07/02/04 22:39 MW 2298553- <br /> Prep Method Pre Date lPr@D Initials Pre Factor <br /> SW30508 0710212004 7:01 ISE 11.00 <br /> Qualifiers: ND1U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> '-Surrogate Recovery Outside Advisable OC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 21 <br />' 719H4 3.6:25 PM <br />