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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> OO HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B5@2.0-2.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-10 <br /> Site: Shell-Tracy Pump P Pum Station <br /> Analyses/Method Result Rep.Llmit Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> Bis(2-ethylhexyl)phthalate ND 330 1 071041041:40 GQ 2301996 <br /> Butyl benzyl phthalate ND 330 1 07/04/04 1:40 GQ 2301996 <br /> Carbazole NO 330 1 071041041:40 GQ 2301996 <br /> Chrysene NO 330 1 071041041:40 GQ 2301996 <br /> Di-n-butyl phthaiate ND 330 1 07/04/04 1:40 GQ 2309996 <br /> Di-n-octyl phthalate NO 330 1 07/04/04 1:40 GQ 2301996 <br /> Dibenz(a,h)anthracene ND 330 1 07/04/04 1:40 GQ 2301996 <br /> Dibenzofuran ND 330 1 071041041:40 GQ 2301996 <br /> Diethyl phthalate ND 330 1 07/04/04 1:40 GQ 2301996 <br /> ' Dimethyl phthalate NO 330 1 07/04/04 1:40 GQ 2301996 <br /> Fluoranthene NO 330 1 071041041:40 GQ 2301996 <br /> Fluorene ND 330 1 071041041:40 GQ 2301996 <br /> Hexachlorobenzene NO 330 1 07/04/04 1:40 GQ 2301996 <br /> Hexachlorobutadiene ND 330 1 071041041:40 GQ 2301996 <br /> Hexachlorocyclopentadiene ND 330 1 071041041:40 GQ 2301996 <br /> Hexachloroethane ND 330 1 071041041:40 GQ 2301996 <br /> ' Indeno(1,2,3-cd)pyrene ND 330 1 07/04/04 1:40 GQ 2301996 <br /> Isophorone NO 330 1 071041041:40 GQ 2301996 <br /> N-Nitrosodi-n-propylamine ND' 330 1 071041041:40 GQ 2309996 <br /> N-Nitrosodiphenylamine ND 330 1 071041041:40 GQ 2301996 <br /> Naphthalene NO 330 1 071041041:40 GQ 2301996 <br /> Nitrobenzene ND 330 1 071041041:40 GQ 2301996 <br /> Pentachlorophenol NO 800 1 071041041:40 GQ _ 2301996 <br /> Phenanthrene NO 330 1 071041041:40 GQ 2301996 <br /> Phenol NO 330 1 071041041:40 GQ 2301996 <br /> Pyrene NO 330 1 071041041:40 GQ 2301996 <br /> Pyridine. NO 330 1 07/04/04 1:40 GO 2301996 <br /> 2-Methylphenol NO 330 1 071041041:40 GQ 2301996 <br /> 3&4-Methylphenol NO 330 1 07/04/04 1:40 GQ 2301996 <br /> Surr:2,4,6-Thbromophenol. 88.1 % 19-135 1 071041041:40 GQ 2301996 <br /> Surr:2-Fluorobiphenyl 52.4 % 15-140 1 07/041041:40 GQ 2301996 <br /> Surr 2-Fluorophenol 56.0 % 15-122 1 071041041:40 GQ 2301996 <br /> Surr:Nitrobenzene-d5 55.3 % 10-134 1 07/04/04 1:40 GQ 2301996 <br /> ' Surr. Phenol-d5 64.0 % 10-123 1 071041041:40 GQ 2301996 <br /> Surr:Terphenyl-d14 64.7 % 18-166 1 07/04/04 1:40 GO 2301996 <br /> 1PreD Method Preo Date 1PreR Initials 1Prep Factor <br /> SW35506 061291200411:24 JOMN 1.p0 <br /> Qualifiers: ND1U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> ' B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> `-Surrogate Recovery Outside Advisable OC Limits Ml-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 23 <br /> trsrva a:or�s ahn <br />