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HOUSTON LABORATORY <br /> ' 8880 INTERCHANGE DRIVE <br /> O HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B5@2.0-2.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-10 <br /> Site: Shell-Tracy Pump Station <br /> ' Analyses/Method Result Rep.Limit DII.Factor QUAL Date Analyzed Analyst Seq.# <br /> VOLATILE ORGANICS BY METHOD 8260B MCL SW8260B Units: uglKg <br /> 1,1.1,2-Tetrachloroethane ND 5 1 06127/04 23:09 ME 2288565 <br /> 1,1,1-Trichloroethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> 1,1,2,2-Tetrachloroethane ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,1,2-Trichloroethane ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,1-Dichloroethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> ' 1,1-Dichloroethene NO 5 1 06/27/04 23:09 ME 2288565 <br /> 1,1-Dichloropropene ND 5 1 06/27/04 23:09 ME2288565 <br /> 1,2.3-Tdchlorobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> ' 1,2,3-Trichloropropane ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2,4-Trichlorobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2,4-Trimethylbenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2-Dibromo-3-chloropropane NO 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2-Dibromoethene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2-Dichlorobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2-Dichloroethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> ' 1,2-Dichioropropane ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1.3,5-Tdmethylbenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,3-Dichlorobenzene NO 5 1 06/27/04 23:09 ME 2288565 <br /> 1,3-Dichloropropane NO 5 1 06/27/04 23:09 ME 2288565 <br /> 1,4-Dichlorobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 2,2-Dichloropropane, ND 5 1 06/27/04 23:09 ME 2288565 <br /> 2-Butanone ND 20 1 06/27/04 23:09 ME 2288565 <br /> 2-Chloroethyl vinyl ether ND 10 1 06/27/04 23:09 ME 2288565 <br /> 2-Chlorotoluene ND 5 1 06127/04 23:09 ME 2288565 <br /> 2-Hexanone NO 10 1 06/27/04 23:09 ME 2288565 <br /> 4-Chlorotoluene ND 5 1 06/27/04 23:09 ME 2288565 <br /> 4-Isopropyltoluene ND 5 1 06127/04 23:09 ME 2288565 <br /> 4-Methyl-2-pentanone ND 10 1 06/27/04 23:09 ME 2288565 <br /> ' Acetone NO 100 1 06/27/04 23:09 ME 2288565 <br /> Acrylonitrile ND 50 1 06/27104 23:09 ME 2288565 <br /> Benzene ND 5 1- 06/27/04 23:09 ME 2288565 <br /> Bromobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Bromochloromethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> Bromodichloromethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> Bromoform ND 5 1 06/27/04 23:09 ME 2288565 <br /> ' Bromomethane ND 10 1 06/27/04 23:09 NSE 2288565 <br /> Carbon disulfide ND 5 1 06/27/04 23:09 ME 2298565 <br /> Carbon tetrachloride ND 5 1 06/27/04 23:09 ME 2288565 <br /> Chlorobenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Chloroethane ND 10 1 06/27/04 23:09 NE 2288565 <br /> Qualifiers: NDIU-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> ' B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> -Surrogate Recovery Outside Advisable QC Limits Mt-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 24 <br /> M04 30627 PM <br />