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HOUSTON LABORATORY <br /> ' 8880 INTERCHANGE DRIVE <br /> ® HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B5@2.0-2.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-10 <br /> Site: Shell-Tracy Pump Station <br /> ' Analyses/Method Result Rep.Limit DII.-Factor QUAL Date Analyzed Analyst Seq.# <br /> Chloroform ND 5 1 06/27/04 23:09 ME 2288565 <br /> Chloromethane .ND 10 1 06/27/04 23:09 ME 2288565 <br /> Dibromochloromethane NO 5 1 06/27/04 23:09 ME 2288565 <br /> Dibromomethane ND 5 1 06/27/04 23:09 ME 2288565 <br /> Dichlorodifluoromethane ND 10 1 06127/04 23:09 ME 2288565 <br /> Ethylbenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Hexachlorobutadiene.. ND 5 1 06/27/04 23:09 ME 2288565 <br /> Isopropyl benzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Methyl tert-butyl ether ND 5 1 06/27/04 23:09 ME 2288565 <br /> ' Methylene chloride ND 5 1 06/27/04 23:09 ME 2288565 <br /> n-Butylbenzene ND 5 1 06/27/04 23:09 IVE 2288565 <br /> n-Propylbenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Naphthalene ND 5 1 06/27/04 23:09 ME 2288565 <br /> . sec-Butylbenzene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Styrene ND 5 1 06/27/04 23:09 ME 2288565 <br /> tert-Butyl benzene ND 5 1 06127/04 23:09 ME 2288565 <br /> ' Tetrachloroethene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Toluene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Trichloroethene ND 5 1 06/27/04 23:09 ME 2288565 <br /> Trichlorofluoromethane ND 5 1 06/27/04 23:09 ME 2288565 <br /> Vinyl acetate ND 10 1 06127/04 23.09 ME 2288565 <br /> Vinyl chloride ND 10 1 06/27/04 23:09 ME 2288565 <br /> cis-1,2-Dichloroethene ND 5 1 06/27/04 23:09 ME 2288565 <br /> cis-1,3-Dichloro propene ND 5 1 06/27/04 23:09 ME 2288565 <br /> m,p-Xylene ND 5 1 06/27/04 23:09 ME 2288565 <br /> o-Xylene ND 5 1 06/27/04 23:09 ME 2288565 <br /> ' trans-1,2-Dichloroethene ND 5 1 06/27/04 23:09 ME 2288565 <br /> trans-1,3-Dichloropropene ND 5 1 0612710423:09 ME 2288565 <br /> Xylenes,Total ND 5 1 06/27/04 23:09 ME 2288565 <br /> 1,2-Dichloroethene(total) ND 5 1 06/27/04 23.09 ME 2288565 <br /> ' Surr: 1,2-Dichloroethane-d4 96.0 % 64-130 1 06/27/04 23:09 ME 2288565 <br /> 5urr:4-Bromofluorobenzene 96.0 % 62-130 1 06/27/04 23:09 ME 2288565 <br /> Sun•:Toluene-d8 88.0 % 70-140 1 06127/0423:09 ME 2288565 <br /> ' Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> -Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 25 <br /> ' 71911043:06 PM <br />