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1534 <br /> llow <br /> CA <br /> McCampbell Analytical, Inc. :www.mccampbse Road,Pittsburg,-maiain@m 65-1701 <br /> f Web:www.mcrampbell.com E-mail:mainQmccampbell.com <br /> "When Quality Counts" I Telephone:877-252-9262 Fax 925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil QC Matrix:. Soil WorkOrder 0805377 <br /> EPA Method SW8015C Extraction SW3550C BatchlD: 35573 Spiked Sample ID: 0805312.003A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD i LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD % Rec. % Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> TPH-Diesel(C 10-C23) 110 20 NR NR NR 108 106 0 70- 130 30 70- 130 30 <br /> 0/.SS: 90 50 92 92 0 94 94 0 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35573 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-OOIA 05/14/08 9:45 AM 05/14/08 05/18/08 3:16 AM 0805377-002A 05/14/08 10:00 AM 05/14/08 05/17/08 9:02 AM <br /> 0805377-003A 05/14/08 10:50 AM 05/14/08 05/18/08 5:33 AM 0805377-004A 05/14/08 11:00 AM 05/14/08 05/16/08 6:11 PM <br /> 0805377-006A 05/14/08 11:30 AM 05/14/08 05/17/08 11:19 AM 0805377-007A 05/14/08 11:40 AM 05/14/08 05/16/08 7:19 PM <br /> 0805377-009A 05/14/08 12:25 PM 05/14/08 05/17/08 1:35 PM 0805377-OIOA 05/14/08 12:40 PM 05/14/08 05/17/08 4:10 AM <br /> 0805377-011A 05/14/08 12:50 PM 05/14/08 05/18/08 12:59 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 JPI QA/QC Officer <br /> 0 <br />