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534 <br /> MCCamubellAnalytical. Inc. www.m1awPassRoad,PE-mair:main@565-1701 <br /> Web:www.mccamphell.com E-mail:mam(rJmccampbell.com <br /> "When Oualitv Counts" I Telephone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> •W.O.Sample Matrix: Soil OC Matrix: Soil - WorkOrder 0805377 <br /> EPA Method SW8015C Extraction SW3550C BatchlD: 35582 Spiked Sample ID: 0805317.012A <br /> Analyte Sample Spiked MS MSD&02 <br /> LCSD _CS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> TPH-Diesel(C 10-C23) ND 20 123 123 109 1.64 70- 130 30 70- 130 30 <br /> %SS: 92 50 118 118 123 18.7 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35582 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-012A 05/14/08 1:45 PM 05/14/08 05/16/088:26 PM 0805377-014A 05/14/08 2:05 PM 05/14/08 05/20/08 1:38 PM <br /> 0805377-015A 05/14/08 2:25 PM 05/14/08 05/17/08 5:1 6AM 0805377-017A 05/14/08 2:50 PM 05/14/08 05/20/08 11:04 PM <br /> 0805377-018A 05/14/08 3:20 PM 05/14/08 05/17/08 3:04 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery,=100`(MSSample)/(Amount Spiked);RPD=100`(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 J2— QA/QC Officer <br /> 0 <br />