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1534 <br /> CA <br /> MCCamnbellAnalytical, Inc. www.mlowPassRoad,PEtmairgain@m 5-1701 <br /> Web:www.mccampbell.wm E-mail:main@m=mpbell.com <br /> "When Oaality Coapts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil QC Matrix: Soil WorkOrder 0805377 <br /> EPA Method SM5520EIF Extraction SM5520E/F EatchID: 35586 Spiked Sample ID: 0805321.00IA <br /> Sample I Spiked I MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(°/) <br /> Analyte <br /> mg/Kg I g/Kg %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> POG 92 1 1000 I III 1 101 1 8.70 1 95 93 1 2.13 1 70- 130 1 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35586 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-OOIA 05/14/08 9:45 AM 05/14/08 05/19/08 4:35 PM 0805377-003A 05/14/08 10:50 AM 05/14/08 05/19/08 4:40 PM <br /> 0805377-006A 05/14/08 11:30 AM 05/14/08 05/19/08 4:45 PM 0805377-009A 05/14/08 12:25 PM 05/14/08 05/19/08 4:50 PM <br /> 0805377-011A 05/14/08 12:50 PM 05/14/08 05/19/08 4:55 PM 0805377-014A 05/14/08 2:05 PM 05/14/08 05/19/08 5:00 PM <br /> 0805377-017A 05/14/08 2:50 PM 05/14/08 05/19/08 5:05 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MSSample)/(Amount Spiked);RPD=100-(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification N° 1644 QA/QC Officer <br /> 0 <br />