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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> McCamubell Analytical, Inc. Web:www.mccmupbell.com E-mail:main@mccampbelLcom <br /> "When OualiW Counts" Telephone:877-252-9262 Pax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8082A <br /> •W.O.Sample Matrix: Soil - QC Matrix: Soil WorkOrder_0805377 <br /> EPA Method SW8082A Extraction SW3550C BatchlD: 35642 Spiked Sample ID: 0805377.00IA <br /> Sample Spiked MS I MSD IMS-MSDI LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> mglkg mglkg %Rec. %Rec. %RPD % Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Aroc1or1260 ND<1.2 0.075 NR NR NR 123 124 0.532 70- 130 20 70- 130 20 <br /> o�SB: 113 0.050 102 105 3.30 97 97 0 70- 130 20 70- 130 20 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35642 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-OOIA 05/14/08 9:45 AM 05/14/08 05/16/08 8:55 PM 0805377-002A 05/14/08 10:00 AM 05/14/08 05/19/08 8:50 PM <br /> 0805377-003A 05/14/08 10:50 AM 05/14/08 05/16/08 9:04 AM 0805377-004A 05/14/08 11:00 AM 05/14/08 05/16/08 11:41 PM <br /> 0805377-006A 05/14/08 11:30 AM 05/14/08 05/17/08 12:37 AM 0805377-007A 05/14/08 11:40 AM 05/14/08 05/15/08 9:02 PM <br /> 0805377-009A 05/14/08 12:25 PM 05/14/08 05/17/08 2:27 AM 0805377-010A 05/14/08 12:40 PM 05/14/08 05/16/08 12:46 AM <br /> 0805377-011A 05/14/08 12:50 PM 05/14/08 05/16/08 1:41 AM 0805377-012A 05/14/08 1:45 PM 05/14/08 05/16/08 2:37 AM <br /> 0805377-014A 05/14/08 2:05 PM 05/14/08 05/20/08 11:27 AM 0805377-015A 05/14/08 2:25 PM 05/14/08 05/17/08 4:18 AM <br /> 0805377-017A 05/14/08 2:50 PM 05/14/08 05/16/08 6:18 AM 0805377-018A 05/14/08 3:20 PM 05/14/08 05/16/08 7:13 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate:RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 J2_ QA/QC Officer <br /> 0 <br />