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Pass <br /> McCamubell Analytical, Inc. 1534Wrcc pbell.w.,Pittsbar:main@ 565-1701 <br /> t Web:www.mccampbell.wm E-mail:main@mccampbell.cory <br /> "When Ouality Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8270C <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0805377 <br /> EPA Method SW8270C Extraction SW3550C BatchlD: 35619 Spiked Sample ID: 0805321-0011A <br /> Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD % Rec. %Rec. %RPD MS I MSD RPD LCS/LCSD RPD <br /> Acenaphthene ND<16 2 84 85.5 1.77 75.6 75.8 0.185 30- 130 30 30- 130 30 <br /> 4-Chloro-3-methylphenoI ND<16 4 104 96.5 7.48 93.9 95.3 1.54 30-130 30 30- 130 30 <br /> 2-Chlorophenol ND<16 4 68.8 70 1.80 91.7 92.6 0.944 30- 130 30 30- 130 30 <br /> 1,4-Dichlorobenzene ND<16 2 85.5 87 1.74 79 M79.2O.20202 30- 130 30 30- 130 302,4-Dinitrotoluene ND<I6 2 48.5 49 1.03 77 77 30- 130 30 30- 130 30 <br /> 4-Nitro henol ND<80 4 NR NR NR 76.4917 30- 130 30 30- 130 30 <br /> N-Nitrosodi-n- ro lamme ND<16 2 NR NR NR 81 35 30- 130 30 30- 130 30 <br /> Pentachlorophenol ND<80 4 NR NR NR 59.9 .4 30- 130 30 30- 130 30 <br /> Phenol ND<16 4 92 77 17.8 99.720 30- 130 30 30- 130 30 <br /> Pyrene ND<16 2 93.5 91.5 2.16 78.7671 30- 130 30 30- 130 30 <br /> 1,2,4-Trichlorobenzene ND<16 2 84 79.5 5.50 82.1427 30- 130 30 30- 130 30 <br /> %SSI: 73 200 87 86 1.27 107 106 0.459 30- 130 30 30- 130 30 <br /> %SS2: 91 200 114 73 43.8,FI 126 126 0 30- 130 30 30- 130 30 <br /> %SS3: 91 200 101 105 3.59 106 104 2.21 30- 130 30 30- 130 30 <br /> %SS4: 98 200 98 98 0 9I 91 0 30- 130 30 30- 130 30 <br /> %SS5: 103 200 103 78 27.2 103 103 0 30- 130 30 30- 130 30 <br /> %SS6: 102 200 102 101 0.682 94 95 1.30 30- 130 30 30- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> Fl =MS/MSD outside of acceptance criteria.LCS-LCSD validate prep batch. <br /> BATCH 35619 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-OOIA 05/14/08 9:45 AM 05/14/08 05/19/08 10:11 AM 0805377-002A 05/14/08 10:00 AM 05/14/08 05/19/08 7:41 AM <br /> 0805377-003A 05/14/08 10:50 AM 05/14/08 05/18/08 11:28 AM 0805377-004A 05/14/08 11:00 AM 05/14/08 05/17/08 10:45 PM <br /> 0805377-006A 05/14/08 11:30 AM 05/14/08 05/19/08 12:16 AM 0805377-007A 05/14/08 11:40 AM 05/14/08 05/18/08 12:02 AM <br /> 0805377-009A 05/14/08 12:25 PM 05/14/08 05/19/08 8:55 AM 0805377-OIOA 05/14/08 12:40 PM 05/14/08 05/18/08 1:18 AM <br /> 0805377-011A 05/14/08 12:50 PM 05/14/08 05/18/08 3:18 PM 0805377-012A 05/14/08 1:45 PM 05/14/08 05/18/08 6:25 AM <br /> 0805377-014A 05/14/08 2:05 PM 05/14/08 05/18/08 5:52 PM 0805377-OISA 05/14/08 2:25 PM 05/14/08 05/18/08 7:41 AM <br /> 0805377-017A 05/14/08 2:50 PM 05/14/08 05/18/08 2:01 PM 0805377-018A 05/14/08 3:20 PM 05/14/08 05/18/08 10:11 AM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Central Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=700-(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> #)surrogate diluted out of range;&=low or no recovery of surrogate or target analytes due to matrix Interference. <br /> 111horatory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels. <br /> 1qW J2- <br /> DHS ELAP Certification No 1644 QA/QC Officer <br />