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' MCCamubell Analytical, Ince 1534WIcca Pass Road,Pittsburg,main@m=mpbell.com <br /> 14;121 <br /> -''1, Web:www.mccampbell.com E-mail:Eanai:maiv@mccampbell.com <br /> ` s' "When(main,Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR E200.8 <br /> W.O.Sample Matrix: water OC Matrix: Water WorkOrder 0805377' <br /> EPA Method E200.8 Extraction E200.8 BatchlD: 35636 Spiked Sample ID: 0805377.026E <br /> MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Sample TSpkd MS MSD <br /> Analyte <br /> pg/L pg/L %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Antimony ND 10 N/A N/A N/A 106 110 3.24 N/A N/A 80- 120 20 <br /> Arsenic 120 10 NR rNR <br /> NR 98.1 100 2.19 70-130 20 80- 120 20 <br /> Barium 2000 100 NR NR 101 104 2.54 70- 130 20 80- 120 20 <br /> Beryllium 3.4 10 N/A N/A 96.4 98.8 2.47 N/A N/A 80- 120 20 <br /> Cadmium 8.4 10 130 4.18 97.8 100 2.58 70-130 20 80- 120 20 <br /> Chromium 190 10 NR NR 100 102 1.48 70- 130 20 80- 120 20 <br /> Cobalt 78 10 NR NR 98.6 100 1.38 70- 130 20 80- 120 20 <br /> Copper 400 10 NR NR NR 104 106 1.90 70-130 20 80- 120 20 <br /> Lead 350 10 NR NR NR 99.6 99.9 0.291 70- 130 20 80- 120 20 <br /> Mercury 0.56 0.25 NR NR NR 104 102 1.86 70- 130 20 80- 120 20 <br /> Molybdenum 6.5 10 90.3 89.4 0.580 94.8 97.7 3.08 70- 130 20 60- 120 20 <br /> Nickel 260 10 NR NR NR 102 103 1.66 70- 130 20 80- 120 20 <br /> Selenium 3.0 10 N/A N/A N/A too 105 4.69 N/A N/A go- 120 20 <br /> Silver 0.84 10 113 108 4.39 103 104 1.74 70- 130 20 80- 120 20 <br /> Thallium 2.7 10 N/A N/A N/A 96.6 98.5 1.99 N/A N/A 80- 120 20 <br /> Vanadium 450 10 NR NR NR 100 102 1.48 70- 130 20 80- 120 20 <br /> 'nc 2900 100 NR NR NR 106 107 1.41 70- 130 20 80- 120 20 <br /> %SS: 99 750 103 100 2.13 93 96 3.95 70- 130 20 70- 130 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100•(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD Spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not applicable to this method. <br /> NR=matrix interference and/or analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high <br /> matrix or analyte content. <br /> dyS ELAP Certification N° 1644 QA/QC Officer <br />