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1534 <br /> McCampbell Analytical. Inc. :www.m1ow Pass Road,PE-mail:main 94565-1701 <br /> Web:www.mccamp6elLcom E-mail:mainCn mccampbelLwm <br /> "When Ouality Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8082A <br /> W.O..Sample Matrix: Water QC Matrix: Water WorkOrder 0805377 <br /> EPA Method SW8082A Extraction SW3510C BatchlD: 35644 Spiked Sample ID: NIA <br /> Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria <br /> Analyte <br /> pg/L pg/L %Rec. %Rec. %RPD % Rec. %Rec. %RPD MS I MSD RPD LCS/LCSD RPD <br /> Aroclor1260 N/A 3.75 N/A N/AN/A 88.2 91.2 3.36 N/A N/A 70- 130 20 <br /> %SSt N/A 2.5 N/A N/A N/A 114 108 5.64 1 N/A N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35644 SUMMARY <br /> Lab ID Dale Sampled Date Extracted Date Analyzed lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805377-020D 05/14/08 4:05 PM 05/14/08 05/19/08 9:45 PM 0805377-021D 05/14/08 4:20 PM 05/14/08 05/17/08 9:48 AM <br /> 0805377-022D 05/14/08 4:45 PM 05/14/08 05/17/08 10:44 AM 0805377-023D 05/14/08 5:00 PM 05/14/08 05/18/08 10:12 AM <br /> 0805377-024D 05/14/08 5:20 PM 05/14/08 05/18/08 11:07 AM 0805377-025D 05/14/08 5:50 PM 05/14/08 05/19/08 10:40 PM <br /> 0805377-026D 05/14/08 6:10 PM 05/14/08 05/20, 3:10 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=700`(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)I((MS+MSD)12). <br /> MS/MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 J2_ QA/QC Officer <br />