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ss <br /> 01 <br /> ' MCCamubell Analytical. Inc. 1534 Willow Pati...Road,PE-mil: ai. 94565-17cl <br /> Web:www.mecampbell.com E-mail:mainQmecampbell.com <br /> y "When Ouality Counts" Tele hone:877-252-9262 Pax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Water QC Matrix: Water WorkOrder 0805377 <br /> EPA Method SW8015C Extraction SW3510C BatchlD: 35612 Spiked Sample ID: NIA <br /> Sample Spiked IVIS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> pg/L pg/L e/Rec. e/Rec. %RPD %Rec. %Rec.I %RPD I MS/MSD I RPD LCS/LCSD RPD <br /> TPH-Diesel(C 10-C23) N/A 1000 N/A N/A N/A 121 121 0 N/A N/A 70- 130 30 <br /> %SS: N/A 1 2500 N/A N/A N/A 117 117 0 N/A N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35612 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab 10 Date Sampled Date Extracted Date Analyzed <br /> 0805377-020A 05/14/08 4:05 PM 05/14/08 05/17/08 6:22 AM 0805377-021A 05/14/08 4:20 PM 05/14/08 05/17/08 9:41 AM <br /> 0805377-022A 05/14/08 4:45 PM 05/14/08 05/17/08 10:48 AM 0805377-023A 05/14/08 5:00 PM 05/14/08 05/17/08 11:55 AM <br /> 0805377-024A 05/14/08 5:20 PM 05/14/08 05/17/08 2:09 PM 0805377-025A 05/14/08 5:50 PM 05/14/08 05/17/08 1:02 PM <br /> 0805377-026A 05/14/08 6:10 PM 05/14/08 05/17/08 1:58 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked):RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance callers due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high melds or analyte content. <br /> 42 <br /> DHS ELAP Certification No 1644 QAIQC Officer <br /> 9 <br />