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MCCamnbell Analytical. lnc. 1534 Wine.Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:main@mccampbell.com <br /> "When Ouallry Counts" I Telephone:877-252-9262 Pax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05;Leamer Date Sampled: 05/15/08 <br /> • 315 W.Pine Street,Suite 8 Date Received: 05/15/08 <br /> Client Contact: Mazda Herbert Date Extracted: 05/15/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/17/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805420-001A 0805420-002A 0805420-003A 0805420-004A Reporting Limit for DF=l; <br /> Client ID B-8-1 B-8-3 B-8-5 B-9-1 ND means not detected <br /> above the reporting limit <br /> Matrix S S S S s w <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/Kg mg/L <br /> ICP-MS Metals,Concentration* <br /> Analvtical Method,6020A Extraction Method: SW30505 Work Order 0805420 <br /> Dilution Factor I 1 I 1 I 1 <br /> Antimonv 8.7 ND ND 15 0.5 NA <br /> Arsenic 28 5.5 8.9 41 0.5 NA <br /> Barium 290 170 180 570 5.0 NA <br /> Beryllium ND 0.70 0.72 ND 0.5 NA <br /> Cadmium 6.4 0.39 ND 15 0.25 NA <br /> Chromium 88 48 63 100 0.5 NA <br /> Cobalt 12 9.7 15 17 0.5 NA <br /> Copper 830 39 43 350 0.5 NA <br /> Lead 440 16 10 1200 0.5 NA <br /> Mercury 0.42 0.076 ND 0.77 0.05 NA <br /> Molybdenum 7.4 2.5 0.69 6.1 0.5 NA <br /> Nickel 130 47 49 130 0.5 NA <br /> • Selenium ND 0.57 ND ND 0.5 NA <br /> Silver 0.78 ND ND 0.62 0.5 NA <br /> Thallium ND ND NDND 0.5 NA <br /> Vanadium 60 84 120 48 0.5 NA <br /> Zinc 1 000 1 8 89 42 5.0 <br /> 2 94 103 93 <br /> Comments <br /> *water samples are reported inµg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,filter samples in tig/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> i)aqueous sample containing greater than-1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery, <br /> caused by matrix interference;nd results are reported on a dry weight basis see attached narrative. <br /> 10V• DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager <br />