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` McCamobell Analytical. Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> 1-1 Web:wwarmccampbell.wm @ <br /> E-mail:mainmccampbell.com <br /> "When Oualiw Counts" I Telephone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05;Learner Date Sampled: 05/15/08 <br /> • 315 W.Pine Street,Suite 8 Date Received: 05/15/08 <br /> Client Contact: Marda Herbert Date Extracted: 05/15/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/17/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805420-005A 0805420-006A 0805420-007A 0805420-008A Reporting Limit for DF-1; <br /> Client ID B-9-5 B-10-1 B-10-5 B-11-I ND means not detected <br /> above the reporting limit <br /> Matrix S S S S s W <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL <br /> ICP-MS Metals,Concentration* <br /> vrcal Method: 6020A Fwaamn Mohnd: SW3050B Work Order: 0805420 <br /> Dilution Factor 1 I 1 1 1 1 <br /> Antimonv ND 9.9 ND ND 0.5 NA <br /> Arsenic 9.1 6.1 2.7 4.4 0.5 NA <br /> Barium 190 210 280 100 5.0 NA <br /> Beryllium 0.54 ND 0.55 NO 0.5 NA <br /> Cadmium ND 5.3 NO ND 0.25 NA <br /> Chromium 50 65 48 23 0.5 NA <br /> Cobalt 12 10 8.5 8.3 0.5 NA <br /> Co per 29 370 30 12 0.5 NA <br /> Lead 7.2 360 7.4 4.1 0.5 NA <br /> Mercury ND 0.61 ND ND 0.05 NA <br /> Molybdenum ND 6.9 ND ND 0.5 NA <br /> Nickel 38 100 37 23 0.5 NA <br /> • Selenium ND ND NO ND 0.5 NA <br /> Silver ND ND NO NO 0.5 NA <br /> Thallium ND ND NO NO 0.5 NA <br /> Vanadium 97 35 63 39 0.5 NA <br /> zin 74 4600 71 7 5.0 <br /> it <br /> a S: 94 93 <br /> Comments <br /> -water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soiUsludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> I)aqueous sample containing greater than-1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;1)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surtrogate recovery, <br /> caused by matrix interference;n results are reported on a dry weight basis see attached narrative. <br /> • DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager <br />