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CA <br /> MCCampbell Analytical, Inc 1534 Willow Pass Road,Pittsburg,-maiain@mc65-1701 <br /> ,tom Web:www.mccamphell.com E-mail:main@mccampbell.com <br /> "When Oualit,Counts' I Telephone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05;Learner Date Sampled: 05/15/08 <br /> • 315 W.Pine Street,Suite 8 Date Received: 05/15/08 <br /> Client Contact: Marda Herbert Date Extracted: 05/15/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/17/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805420-009A 0805420-OIOA 0805420-01 IA 0805420-012A Reposing Limit for DF=1; <br /> Client LD B-11-5 B-12-1 B-12-5 B-13-1 ND means not detected <br /> above the reposing limit <br /> Matrix S S S S s W <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/Kg mg/L <br /> ICP-MS Metals,Concentration* <br /> vic (Method6020A Extraction Method: SW3050B W rk Or er Q805420 <br /> Dilution Factor I 1 1 I I I <br /> Anlimonv ND 2.8 0.51 530 0.5 NA <br /> Arsenic 41 6.3 5.0 88 0.5 NA <br /> Barium 340 250 120 1400 5.0 NA <br /> Beryllium ND ND 0.50 ND 0.5 NA <br /> Cadmium ND 1.5 ND 55 0.25 NA <br /> Chromium 41 39 40 2500 0.5 NA <br /> Cobalt 21 12 8.7 88 0.5 NA <br /> Copper 26 100 27 7900 0.5 NA <br /> Lead 6.5 160 1 8.4 19,000 0.5 1 NA <br /> Mercury ND 0.22 ND 8.8 0.05 NA <br /> Molybdenum 0.98 2.4 0.52 260 0.5 NA <br /> Nickel 34 47 32 1200 0.5 NA <br /> • Selenium ND ND ND 1.7 0.5 NA <br /> Silver ND ND ND 32 0.5 NA <br /> Thallium ND ND ND 6.7 0.5 NA <br /> Vanadium 86 52 62 130 0.5 NA <br /> Zinc90 29.000 NA <br /> %SS: 5 2 94 98 <br /> Comments <br /> -water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,wil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in lig/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water, <br /> it aqueous sample containing greater than-1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery, <br /> caused by matrix interference;n results are reported on a dry weight basis see attached narrative. <br /> • DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager <br />