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MCC ampbell Analytical,Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Tt Web:www.mccampbelLcom E-mail:maintr?imceampbell.com <br /> "When Ouality Counts" I Tele hone:877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil QC Matrix: Soil - WorkOrder 0805420 <br /> EPA Method SM5520EIF Extraction SM5520EIF BatchlD: 35586 Spiked Sample ID: 0805321-001A <br /> Analyte Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec.I%Rec. .RPD %Rec. %Rec. %RPD I MS/MSD RPD I LCS/LCSD I RPD <br /> POG 92 1000 111 1 101 1 8.70 1 95 1 93 2.13 170- 130 30 1 70- 130 1 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35586 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805420-OOIA 05/15/08 10:15 AM 05/15/08 05/19/08 5:15 PM 0805420-002A 05/15/08 10:25 AM 05/15/08 05/19/08 5:20 PM <br /> 0805420-004A 05/15/08 10:45 AM 05/15/08 05/19/08 5:25 PM 0805420-006A 05/15/08 11:30 AM 05/15/08 05/19/08 5:30 PM <br /> 0805420-008A 05/15/08 1135 AM 05/15/08 05/19/08 5:35 PM 0805420-OIOA 05/15/08 12:10 PM 05/15/08 05/19/08 5:40 PM <br /> 0805420-OI2A 05/15/08 1:45 PM 05/15/08 05/19/08 5:45 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteda due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 QA/QC Officer <br /> • <br />