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McCamnbell Analytical. Inc. 1534 Willow,Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.m=mpbeli.com E-mail:main@mcoampbell.com <br /> When Ouality Counts' I Telephone:877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8082A <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0805420 <br /> EPA Method SW8082A Extraction SW3550C BatchlD: 35642 Spiked Sample ID: 0805377-001A <br /> Analyte Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mglkg mg/kg a/Rec. %Rec. %RPD % Rec. %Rec. %RPD IMS/MSD RPD LCS/LCSD RPD <br /> Aroclor1260 ND<l.2 0.075 NR NR NR 123 124 0.532 70- 130 20 70- 130 20 <br /> %SS: 113 0.050 102 105 3.30 97 97 0 70- 130 20 70- 130 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35642 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805420-OOIA - 05/15/08 10:15 AM 05/15/08 05/21/08 8:45 PM 0805420-002A 05/15/08 10:25 AM 05/15/08 05/21/08 9:40 PM <br /> 0805420-003A 05/15/08 10:30 AM 05/15/08 05/20/08 4:09 AM 0805420-004A 05/15/08 10:45 AM 05/15/08 05/20/08 5:03 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 J12— QA/QC Officer <br /> 0 <br />