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1534 <br /> McCamubell Analyticaljnc. :www.mc1 mpbsll.com Pittsburg,main@=ampbell.com Web:www.mccampbell.com E-mail:maviQmccamphell.com <br /> "When Ouality Counts" I Telephone,877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8082A <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0805420 <br /> EPA Method SW8082A Extraction SW3550C BatchlD: 35675 Spiked Sample ID: 0805420.013A <br /> Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> mg/kg mg/kg %Rae. %Rec. %RPD % Rec. a/Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Aroclor1260 ND 0.075 193F1 194FI 1.85 126 125 0.531 70- 130 1 20 70- 130 20 <br /> -/.SS: 99 0.050 119 123 3.76 82 81 0.590 70- 130 1 20 1 70- 130 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> F1=MS/MSD outside of acceptance criteria.LCS-LCSD validate prep batch. <br /> BATCH 35675 SUMMARY <br /> Lab ID Date Sampled Date Extracted Dale Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805420-005A 05/15/08 10:55 AM 05/15/08 05/17/08 12:20 PM 0805420-006A 05/15/08 11:30 AM 05/15/08 05/17/08 1:16 PM <br /> 0805420-007A 05/15/08 11:40 AM 05/15/08 05/17/08 2:14 PM 0805420-008A 05/15/08 11:35 AM 05/15/08 05/17/08 3:10 PM <br /> 0805420-009A 05/15/08 12:00 PM 05/15/08 05/17/08 5:04 PM 0805420-0IOA 05/15/08 12:10 PM 05/15/08 05/20/08 5:57 AM <br /> 0805420-OIIA 05/15/08 1:15 PM 05/15/08 05/19/08 5:30 AM 0805420-012A 05/15/08 1:45 PM 05/15/08 05/21/08 10:35 PM <br /> 0805420-013A 05/15/08 2:05 PM 05/15/08 05/18/08 9:18 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=not enough sample to perforin matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification N° 1644 QA/QC Officer <br /> 0 <br />