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1534 W illow Pass Road,Pittsburg,CA 94565-1701 <br /> McCamubell Analytical, Inc. Web:www.mccampbell.com E-mail:mainQmccampbell.com <br /> "When Ouali[v Counts" Tele hone:877-252-9262 Pax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/16/08 <br /> • LEARNER,2711 Navy Dr.,Stockton,Ca Date Received 05/16/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Mazda Herbert Date Extracted 05/16/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/20/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805464-OOIA 0805464-002A 0805464-003A 0805464-004A Reporting Limit for DF-1; <br /> Client ID B-14-1 B-14-5 B-15-1 B-15-5 ND means at detected <br /> above the reporting limit <br /> Matrix S S S S s W <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/Kg mg/L <br /> ICP-MS Metals,Concentration* <br /> nalvtical Meth ' 6020A Ex radion Method: SW3050B W rk Order 4 <br /> Dilution Factor 1 1 I 1 1 1 1 <br /> Antimony 0.73 ND 1.3 NO N5.0 <br /> NA <br /> Arsenic 7.4 32 6.9 3.9 NA <br /> Barium 200 320 140 170 NA <br /> Beryllium 0.72 0.53 ND ND NA <br /> Cadmium 0.50 ND 0.76 ND NA <br /> Chromium 60 47 31 41 NA <br /> Cobalt 13 19 8.3 14 NA <br /> Copper 51 31 59 25 0.5 NA <br /> Lead 27 8.1 63 6.7 0.5 NA <br /> Mercury 0.16 ND 0.24 NO 0.05 NA <br /> Molybdenum 2.7 1.2 1.4 0.85 0.5 NA <br /> Nickel 56 38 33 30 0.5 NA <br /> Selenium NO ND NO NO 0.5 NA <br /> Silver ND NO NO NO 0.5 NA <br /> Thallium ND ND ND ND 0.5 NA <br /> Vanadium 80 120 42 69 0.5 1 NA <br /> Zin 150 71 560 1 55 1 5wO I NA <br /> ° SS: 98 98 97 1 10 <br /> Comments <br /> -water samples are reported in gg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> i)aqueous sample containing greater than—1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery, <br /> caused by matrix interference,n results are reported on a dry weight basis see attached narrative. <br /> DHS ELAP Certification N° 1644 Angela Rydelius,Lab Manager <br />