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McCamnbell Analytical, Inc. 1534Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:mainrLJmccampbell.mm <br /> 14 "When Ouality Counts" I Telephone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/16/08 <br /> LEARNER,2711 Navy Dr.,Stockton,Ca Date Received 05/16/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Marda Herbert Date Extracted 05/16/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/20/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805464-005A 0805464-006A 0805464-007A 0805464-008A Reporting Limit for DF=1; <br /> Client ID B-16-1 B-16-5 B-17-1 B-17-5 NDmeansnotdetecied <br /> above the"porting limit <br /> Matrix S S S S s W <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/Kg mWL <br /> ICP-MS Metals,Concentration* <br /> Analytical Mctlmd: 6020A fixtr [ion Method: SW3050B Work Order: 4 4 <br /> Dilution Factor 1 I I I I <br /> Antimony 5.9 ND 1.3 0.64 0.5 NA <br /> Arsenic 5.3 6.3 4.7 16 0.5 NA <br /> Barium 180 470 110 220 5.0 NA <br /> Beryllium ND 0.67 ND 0.53 0.5 NA <br /> Cadmium 3.7 ND 0.64 0.26 0.25 NA <br /> Chromium 400 51 33 46 0.5 NA <br /> Cobalt 14 1 20 8.1 16 0.5 NA <br /> Cooper 480 36 71 43 0.5 NA <br /> Lead 280 9.9 190 21 0.5 NA <br /> Mercury 0.24 ND 0.12 ND 0.05 NA <br /> Molybdenum II 0.64 1.2 0.74 0.5 NA <br /> Nickel 290 42 36 38 0.5 NA <br /> Selenium ND ND NO ND 0.5 NA <br /> Silver ND ND ND NO 0.5 NA <br /> Thallium ND ND ND ND 0.5 NA <br /> Vanadium 49 95 43 100 0.5 NA <br /> Zto 5200 1990 250 5.0 NA <br /> %SS: 9ft 0o 80 96 <br /> Comments <br /> *water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soiVsludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> i)aqueous sample containing greater than-1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery, <br /> caused by matrix interference,n results are reported on a dry weight basis see attached narrative. <br /> JP <br /> DHS ELAP Certification NO 1644 Angela Rydelius,Lab Manager <br />